N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester

Base Information

• Chemical Name: N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester
• CAS No.: 955362-50-2
• Molecular Formula: C₁₃H₁₉N₃O₂S
• Molecular Weight: 0

Synonyms:N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester

Chemical Property of N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester

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Technology Process of N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester

There total 1 articles about N-[4-[[(methylamino)thioxomethyl]amino]phenyl]carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (4-isothiocyanatophenyl)carbamate (89631-75-4) + methylamine (74-89-5) → 1,1-dimethylethyl (4-{[(methylamino)carbonothioyl]amino}phenyl)carbamate (955362-50-2)

Guidance literature:

In ethanol; at 20 ℃; for 1h;

Reference yield:

1,1-dimethylethyl (4-{[(methylamino)carbonothioyl]amino}phenyl)carbamate (955362-50-2) + 3-chloropentane-2,4-dione (1694-29-7) → 1-{2-[(4-tert-butoxycarbonylaminophenyl)imino]-3,4-dimethyl-2,3-dihydro-1,3-thiazol-5-yl}ethanone (955362-47-7)

Guidance literature:

In ethanol; at 100 ℃; for 0.333333h; Microwave irradiation;

Reference yield:

1,1-dimethylethyl (4-{[(methylamino)carbonothioyl]amino}phenyl)carbamate (955362-50-2) + 3-chloropentane-2,4-dione (1694-29-7) → 1-{2-[(4-aminophenyl)imino]-3,4-dimethyl-2,3-dihydro-1,3-thiazol-5-yl}ethanone (955362-07-9) + 1-{2-[(4-tert-butoxycarbonylaminophenyl)imino]-3,4-dimethyl-2,3-dihydro-1,3-thiazol-5-yl}ethanone (955362-47-7)

Guidance literature:

In ethanol; at 100 ℃; for 0.333333h; Product distribution / selectivity; Microwave irradiation;

upstream raw materials:

tert-butyl (4-isothiocyanatophenyl)carbamate

methylamine

Downstream raw materials:

1-{2-[(4-tert-butoxycarbonylaminophenyl)imino]-3,4-dimethyl-2,3-dihydro-1,3-thiazol-5-yl}ethanone

1-{2-[(4-aminophenyl)imino]-3,4-dimethyl-2,3-dihydro-1,3-thiazol-5-yl}ethanone

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