Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester

Base Information

Chemical Name:Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester
CAS No.:5211-17-6
Molecular Formula:C29H50OS2
Molecular Weight:478.847
Hs Code.:
Mol file:5211-17-6.mol

Synonyms:Carbonodithioic acid O-(5α-cholestan-3β-yl) S-methyl ester;Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester

Suppliers and Price of Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester

Chemical Property:

Boiling Point:542.6±17.0 °C(Predicted)
PSA：66.62000
Density:1.04±0.1 g/cm3(Predicted)
LogP:9.14080

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester

There total 9 articles about Dithiocarbonic acid O-(5α-cholestan-3β-yl) S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-15-0,12122-00-8
carbon disulfide

: 80-97-7
Cholestanol

: 74-88-4
methyl iodide

: 5211-17-6
3β-(methylthio)thiocarbonyloxy-5α-cholestane

Guidance literature:: Cholestanol; With 1H-imidazole; sodium hydride; In tetrahydrofuran; for 3h; Heating;

carbon disulfide; In tetrahydrofuran; for 0.5h; Heating;

methyl iodide; In tetrahydrofuran; for 1h; Heating;
DOI:10.1002/mrc.1635

Reference yield:

: 80-97-7
Cholestanol

: 5211-17-6
3β-(methylthio)thiocarbonyloxy-5α-cholestane

Guidance literature:: With carbon disulfide; sodium hydride; benzene; anschliessend Erwaermen mit CH₃I;
DOI:10.1021/ja01141a069

Reference yield:

: 98569-97-2
S-isopropyl-O-3β-cholestanyldithiocarbonate

: 74-88-4
methyl iodide

: 5211-17-6
3β-(methylthio)thiocarbonyloxy-5α-cholestane

Guidance literature:: With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile); Yield given. Multistep reaction; 1.) C₆D₆, 80 deg C, 2.) MeI, RT, 18 h;
DOI:10.1016/S0040-4020(01)90612-X