Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI)

Base Information

• Chemical Name: Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI)
• CAS No.: 213757-85-8
• Molecular Formula: C₇H₁₁NO₃
• Molecular Weight: 157.169
• Mol file: 213757-85-8.mol

Synonyms:Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI)

Chemical Property of Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI)

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Technology Process of Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI)

There total 2 articles about Cyclopropanecarboxylic acid, 2-[(acetylamino)methyl]-, (1R,2R)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1R,2S)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid ethyl ester → (1S,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (213757-85-8)

Guidance literature:

With hydrogenchloride; In acetic acid; Ambient temperature;

DOI:10.1016/S0957-4166(98)00250-X

Reference yield: 90.0%

(1R,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid ethyl ester → (1R,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (213757-85-8)

Guidance literature:

With hydrogenchloride; In acetic acid; Ambient temperature;

DOI:10.1016/S0957-4166(98)00250-X

Reference yield: 17.0%

(1R,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (213757-85-8) + (R)-Pantolacton (599-04-2) → (1R,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester + (1S,2S)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester (213757-87-0)

Guidance literature:

With dicyclohexyl-carbodiimide; In acetonitrile; Heating;

DOI:10.1016/S0957-4166(98)00250-X

Downstream raw materials:

(1R,2S)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

(1S,2R)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

(1S,2S)-2-(Acetylamino-methyl)-cyclopropanecarboxylic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

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