1,4-Dihydropyridine-1-carboxylic acid methyl ester

Base Information

Chemical Name:1,4-Dihydropyridine-1-carboxylic acid methyl ester
CAS No.:33707-37-8
Molecular Formula:C7H9NO2
Molecular Weight:139.154
Hs Code.:
Mol file:33707-37-8.mol

Synonyms:1,4-Dihydropyridine-1-carboxylic acid methyl ester;Pyridine-1(4H)-carboxylic acid methyl ester

Suppliers and Price of 1,4-Dihydropyridine-1-carboxylic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1,4-Dihydropyridine-1-carboxylic acid methyl ester

Chemical Property:

PSA：29.54000
LogP:1.42380

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Dihydropyridine-1-carboxylic acid methyl ester

There total 4 articles about 1,4-Dihydropyridine-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 66893-72-9
methyl 2,6-dimethoxy-1-piperidinecarboxylate

: 33707-37-8
1-methoxycarbonyl-1,4-dihydropyridine

Guidance literature:: With ammonium chloride; for 5h; under 50 Torr; Heating;
DOI:10.1021/ja00388a037

Reference yield: 63.0%

: 110-86-1
pyridine

: 79-22-1
methyl chloroformate

: 33707-37-8
1-methoxycarbonyl-1,4-dihydropyridine

: 33707-36-7
1-(methoxycarbonyl)-1,2-dihydropyridine

Guidance literature:: With sodium tetrahydroborate; In methanol; diethyl ether; at -78 ℃; for 2h; Title compound not separated from byproducts;

Reference yield:

: 1796-27-6
piperidine-1-carboxylic acid methyl ester

: 33707-37-8
1-methoxycarbonyl-1,4-dihydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / anodic oxidation in tetraethylammonium p-toluenesulfonate

2: 86 percent / NH₄Cl / 5 h / 50 Torr / Heating

With ammonium chloride;
DOI:10.1021/ja00388a037