METHYL PIPERIDINE-1-CARBOXYLATE

Base Information

• Chemical Name: METHYL PIPERIDINE-1-CARBOXYLATE
• CAS No.: 1796-27-6
• Molecular Formula: C7H13 N O2
• Molecular Weight: 143.186
• Hs Code.: 2933399090
• Mol file: 1796-27-6.mol

Synonyms:1-(Methoxycarbonyl)piperidine;Methyl 1-piperidinecarboxylate; N-(Carbomethoxy)piperidine;N-(Methoxycarbonyl)piperidine; NSC 30494; NSC 40881

Chemical Property of METHYL PIPERIDINE-1-CARBOXYLATE

Chemical Property:

• Vapor Pressure: 0.369mmHg at 25°C
• Boiling Point: 197.9°C at 760 mmHg
• PKA: -1.34±0.20(Predicted)
• Flash Point: 73.5°C
• PSA: 29.54000
• Density: 1.059g/cm³
• LogP: 1.17660
• Storage Temp.: Refrigerator, under inert atmosphere
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

99%, ^*data from raw suppliers

MethylPiperidine-1-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of METHYL PIPERIDINE-1-CARBOXYLATE

There total 37 articles about METHYL PIPERIDINE-1-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

piperidine (110-89-4) + methanol (67-56-1) + carbon monoxide (201230-82-2) → piperidine-1-carboxylic acid methyl ester (1796-27-6)

Guidance literature:

With 2C₇H₉N₄*Au⁽¹⁺⁾*Cu⁽¹⁺⁾*2I^(1-); In toluene; at 90 ℃; for 24h; Time; Autoclave;

DOI:10.1002/anie.201914089

Reference yield: 90.0%

piperidine (110-89-4) + carbonic acid dimethyl ester (616-38-6) → piperidine-1-carboxylic acid methyl ester (1796-27-6)

Guidance literature:

With aluminum oxide; for 48h; Heating;

DOI:10.1016/S0040-4039(00)01051-0

Reference yield: 90.0%

piperidine (110-89-4) + methyl chloroformate (79-22-1) → piperidine-1-carboxylic acid methyl ester (1796-27-6)

Guidance literature:

With base;

DOI:10.1021/ja00395a029

upstream raw materials:

piperidine

methyl chloroformate

methanol

piperidine carbamoyl chloride

Downstream raw materials:

N-methylcyclohexylamine

3,4-dihydro-2H-pyridine-1-carboxylic acid methyl ester

2-hydroxy-1-methoxycarbonylpiperidine

methyl 2-(2-propenyl)piperidinecarboxylate

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