Ethanone,1-(2-amino-5-iodo-3-methylphenyl)-

Base Information

• Chemical Name: Ethanone,1-(2-amino-5-iodo-3-methylphenyl)-
• CAS No.: 935292-72-1
• Molecular Formula: C9H10INO
• Molecular Weight: 275.09
• Hs Code.: 2922399090
• Mol file: 935292-72-1.mol

Synonyms:Ethanone,1-(2-amino-5-iodo-3-methylphenyl)-;1-(2-Amino-5-iodo-3-methylphenyl)-ethanone

Chemical Property of Ethanone,1-(2-amino-5-iodo-3-methylphenyl)-

Chemical Property:

• Melting Point: 165～168℃
• PSA: 43.09000
• LogP: 2.96560

Purity/Quality:

97% ^*data from raw suppliers

1-(2-Amino-5-iodo-3-methylphenyl)-1-ethanone >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone,1-(2-amino-5-iodo-3-methylphenyl)-

There total 1 articles about Ethanone,1-(2-amino-5-iodo-3-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N-(2-acetyl-4-iodo-6-methylphenyl)-2,2,2-trifluoroacetamide (935292-71-0) → 1-(2-amino-5-iodo-3-methylphenyl)ethanone (935292-72-1)

Guidance literature:

With methanol; sodium hydroxide;

DOI:10.1016/j.bmcl.2009.11.010

Reference yield: 80.0%

pyrrolidine (123-75-1) + 1-(2-amino-5-iodo-3-methylphenyl)ethanone (935292-72-1) → 1-{5-iodo-3-methyl-2-[1-pyrrolidinyldiazenyl]phenyl}ethanone (935292-75-4)

Guidance literature:

1-(2-amino-5-iodo-3-methylphenyl)ethanone; With hydrogenchloride; sodium nitrite; In tetrahydrofuran; water;

pyrrolidine; With potassium carbonate; In tetrahydrofuran; water;

DOI:10.1016/j.bmcl.2009.11.010

Reference yield: 77.0%

1-(2-amino-5-iodo-3-methylphenyl)ethanone (935292-72-1) + tryptamine (61-54-1) → C19H20N3I

Guidance literature:

With iodine; In ethanol; at 20 ℃; for 9h;

DOI:10.1016/j.tetlet.2007.06.099

upstream raw materials:

N-(2-acetyl-4-iodo-6-methylphenyl)-2,2,2-trifluoroacetamide

Downstream raw materials:

1-{5-iodo-3-methyl-2-[1-pyrrolidinyldiazenyl]phenyl}ethanone

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