3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester

Base Information

• Chemical Name: 3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester
• CAS No.: 16632-06-7
• Molecular Formula: C₁₆H₁₄O₆
• Molecular Weight: 302.284
• Mol file: 16632-06-7.mol

Synonyms:3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester

Chemical Property of 3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester

Chemical Property:

• PSA: 93.06000
• LogP: 2.33800

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester

There total 2 articles about 3,5-Dihydroxy-2,4-biphenyldicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,3-diacetoxyacetone (6946-10-7) + phenylpropynoic acid methyl ester (4891-38-7) → Dimethyl 2,4-dihydroxy-6-phenylbenzene-1,3-dicarboxylate (16632-06-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 55 ℃; for 3.5h;

DOI:10.1080/00397919808004454

Reference yield:

→ Dimethyl 2,4-dihydroxy-6-phenylbenzene-1,3-dicarboxylate (16632-06-7)

Guidance literature:

Phenyl-dipyron, methanol. KOH; (neben anderen Verbindungen);

DOI:10.1139/v67-317

upstream raw materials:

1,3-diacetoxyacetone

phenylpropynoic acid methyl ester

Refernces