1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate

Base Information

• Chemical Name: 1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate
• CAS No.: 1403767-29-2
• Molecular Formula: C₁₂H₁₉FO₄
• Molecular Weight: 246.279
• Hs Code.: 2917200090
• Mol file: 1403767-29-2.mol

Synonyms:1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate

Chemical Property of 1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Diisopropyl3-Fluorocyclobutane-1,1-dicarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate

There total 2 articles about 1,1-bis(propan-2-yl) 3-fluorocyclobutane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

dipropan-2-yl 3-hydroxycyclobutane-1,1-dicarboxylate (869109-31-9) → diisopropyl 3-fluorocyclobutane-1,1-dicarboxylate (1403767-29-2)

Guidance literature:

With morpholinosulfur trifluoride; In dichloromethane; at 0 - 20 ℃; for 40h;

DOI:10.1002/ejoc.202100804

Reference yield:

dipropan-2-yl 3-oxocyclobutane-1,1-dicarboxylate (893724-10-2) → diisopropyl 3-fluorocyclobutane-1,1-dicarboxylate (1403767-29-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium tetrahydroborate; water / tetrahydrofuran / 1 h / 0 - 5 °C

2: morpholinosulfur trifluoride / dichloromethane / 40 h / 0 - 20 °C

With sodium tetrahydroborate; water; morpholinosulfur trifluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/ejoc.202100804

upstream raw materials:

dipropan-2-yl 3-hydroxycyclobutane-1,1-dicarboxylate

dipropan-2-yl 3-oxocyclobutane-1,1-dicarboxylate

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