4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide

Base Information

Chemical Name:4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide
CAS No.:156900-59-3
Molecular Formula:C₁₄H₁₉NO₂S
Molecular Weight:265.376
Hs Code.:
European Community (EC) Number:689-474-3
DSSTox Substance ID:DTXSID90576128
Mol file:156900-59-3.mol

Synonyms:156900-59-3;4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide;4-METHYL-N-(5-METHYLHEXA-3,4-DIEN-1-YL)BENZENESULFONAMIDE;starbld0020468;DTXSID90576128;N-Tosyl-5-methyl-3,4-hexadienylamine, 95%

Suppliers and Price of 4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:265.11365002
Heavy Atom Count:18
Complexity:402

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NCCC=C=C(C)C

Technology Process of 4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide

There total 4 articles about 4-Methyl-N-(5-methylhexa-3,4-dien-1-yl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: Methanesulfonic acid 5-methyl-hexa-3,4-dienyl ester

: 70-55-3
toluene-4-sulfonamide

: 156900-59-3
5-methyl-N-(p-tosyl)hexa-3,4-dien-1-amine

Guidance literature:: With potassium carbonate; In acetonitrile; for 16h; Reflux; Inert atmosphere;
DOI:10.1021/ol201041h

Reference yield:

: 30333-01-8
5-methylhexa-3,4-dienoic acid ethyl ester

: 156900-59-3
5-methyl-N-(p-tosyl)hexa-3,4-dien-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere

2: triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3: potassium carbonate / acetonitrile / 16 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ol201041h

Reference yield:

: 115-19-5
2-methyl-but-3-yn-2-ol

: 156900-59-3
5-methyl-N-(p-tosyl)hexa-3,4-dien-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 3.33 h / 20 - 145 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere

3: triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4: potassium carbonate / acetonitrile / 16 h / Reflux; Inert atmosphere

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; acetonitrile;
DOI:10.1021/ol201041h