1-Chloronaphtho[2,1-b]thiophene

Base Information

Chemical Name:1-Chloronaphtho[2,1-b]thiophene
CAS No.:85992-26-3
Molecular Formula:C12H7ClS
Molecular Weight:218.707
Hs Code.:2934999090
DSSTox Substance ID:DTXSID701305200
Mol file:85992-26-3.mol

Synonyms:1-chloronaphtho[2,1-b]thiophene;85992-26-3;DTXSID701305200

Suppliers and Price of 1-Chloronaphtho[2,1-b]thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-CHLORONAPHTHO[2,1-B]THIOPHENE 95.00%
5MG
$ 504.12

Total 3 raw suppliers

Chemical Property of 1-Chloronaphtho[2,1-b]thiophene

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:373.234°C at 760 mmHg
Flash Point:235.624°C
PSA：28.24000
Density:1.375g/cm³
LogP:4.70790
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:217.9956991
Heavy Atom Count:14
Complexity:218

Purity/Quality:: 1-CHLORONAPHTHO[2,1-B]THIOPHENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C(=CS3)Cl

Technology Process of 1-Chloronaphtho[2,1-b]thiophene

There total 2 articles about 1-Chloronaphtho[2,1-b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 85589-69-1
3-chloro-2-carboxynaphtho<2,1-b>thiophene

: 85992-26-3
3-chloronaphtho<2,1-b>thiophene

Guidance literature:: With copper; In quinoline; for 5h; Heating;
DOI:10.1007/BF00506424

Reference yield:

: 85992-25-2
1-chloronaphtho<2,1-b>thiophene-2-carboxoyl chloride

: 85992-26-3
3-chloronaphtho<2,1-b>thiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaOH / ethanol; H₂O / 6 h / Heating

2: 54 percent / powdered copper / quinoline / 5 h / Heating

With sodium hydroxide; copper; In quinoline; ethanol; water;
DOI:10.1007/BF00506424