8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE

Base Information

• Chemical Name: 8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE
• CAS No.: 135692-39-6
• Molecular Formula: C₁₃H₁₃NOS₃
• Molecular Weight: 295.45
• Hs Code.: 2933990090
• Mol file: 135692-39-6.mol

Synonyms:8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE;AKOS BBS-00005655;ASISCHEM N45085;TIMTEC-BB SBB001213;1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE, 4,5-DIHYDRO-8-METHOXY-4,4-DIMETHYL-;4,5-DIHYDRO-8-METHOXY-4,4-DIMETHYL-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE

Chemical Property of 8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE

Chemical Property:

• Boiling Point: 490.3±55.0 °C(Predicted)
• PKA: 2.23±0.40(Predicted)
• PSA: 109.83000
• Density: 1.42±0.1 g/cm3(Predicted)
• LogP: 5.01330

Purity/Quality:

98%min ^*data from raw suppliers

8-Methoxy-4,4-dimethyl-4,5-dihydro-1H-[1,2]dithiolo[3,4-c]quinoline-1-thione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE

There total 1 articles about 8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

6-methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline (4053-50-3) → 4,5-dihydro-4,4-dimethyl-8-methoxy-2,3-dithiolo<5,4c>quinoline-1-thione (135692-39-6)

Guidance literature:

With sulfur; In N,N-dimethyl-formamide; for 8h; Heating;

DOI:10.1007/BF00958554

Reference yield: 71.0%

4,5-dihydro-4,4-dimethyl-8-methoxy-2,3-dithiolo<5,4c>quinoline-1-thione (135692-39-6) + dimethyl acetylenedicarboxylate (762-42-5) → 2-(6-methoxy-2,2-dimethyl-3-thioxo-2,3-dihydro-1H-quinolin-4-ylidene)-[1,3]dithiole-4,5-dicarboxylic acid dimethyl ester

Guidance literature:

In chloroform; at 20 ℃; for 30h;

DOI:10.1007/BF02324643

Reference yield: 68.0%

4,5-dihydro-4,4-dimethyl-8-methoxy-2,3-dithiolo<5,4c>quinoline-1-thione (135692-39-6) + dimethyl acetylenedicarboxylate (762-42-5) → C25H25NO9S3

Guidance literature:

In benzene; for 15h; Heating;

DOI:10.1007/BF02324643

upstream raw materials:

6-methoxy-2,2,4-trimethyl-1,2-dihydro-quinoline

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