BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride)

Base Information

• Chemical Name: BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride)
• CAS No.: 328933-65-9
• Molecular Formula: C15H24ClNO2
• Molecular Weight: 285.814
• Mol file: 328933-65-9.mol

Synonyms:BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride);4-(2-Azepan-1-ylethoxy)benzyl alcohol hydrochloride;(4-(2-(azepan-1-yl)ethoxy)phenyl)Methanol HCl

Chemical Property of BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride)

Chemical Property:

• PSA: 32.70000
• LogP: 3.17360

Purity/Quality:

99%, ^*data from raw suppliers

(4-(2-(Azepan-1-yl)ethoxy)phenyl)methanolhydrochloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride)

There total 1 articles about BenzeneMethanol, 4-[2-(hexahydro-1H-azepin-1-yl)ethoxy]- (hydrochloride) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[4-(2-hexamethyleneimino-1-yl-ethoxy)-phenyl]-methanol (223251-16-9) → (4-(2-(azepan-1-yl)ethyl)phenyl)methanol hydrochloride (328933-65-9)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 0 - 10 ℃;

Reference yield: 85.0%

(4-(2-(azepan-1-yl)ethyl)phenyl)methanol hydrochloride (328933-65-9) → 1-(2-[4-(bromomethyl)phenoxy]ethyl)azepane hydrobromide

Guidance literature:

With phosphorus tribromide; In dichloromethane; at -15 - 20 ℃;

Reference yield:

(4-(2-(azepan-1-yl)ethyl)phenyl)methanol hydrochloride (328933-65-9) → 1-{2-[4-(chloromethyl)phenoxy]ethyl}hexahydro-1H-azepine hydrochloride (223251-25-0)

Guidance literature:

With thionyl chloride; at 50 ℃;

upstream raw materials:

[4-(2-hexamethyleneimino-1-yl-ethoxy)-phenyl]-methanol

Downstream raw materials:

1-{2-[4-(chloromethyl)phenoxy]ethyl}hexahydro-1H-azepine hydrochloride

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