3-Methoxynaphthalene-1-carboxylic acid

Base Information

Chemical Name:3-Methoxynaphthalene-1-carboxylic acid
CAS No.:147397-60-2
Molecular Formula:C12H10O3
Molecular Weight:202.206
Hs Code.:
European Community (EC) Number:868-640-0
DSSTox Substance ID:DTXSID10598807
Nikkaji Number:J2.307.279C
Wikidata:Q82494609
Mol file:147397-60-2.mol

Synonyms:3-Methoxynaphthalene-1-carboxylic acid;147397-60-2;3-methoxy-1-naphthoic acid;SCHEMBL1162404;DTXSID10598807;MFCD17012515;AT22270;AS-76936;SY283527;DB-083980;CS-0134840;EN300-7540422

Suppliers and Price of 3-Methoxynaphthalene-1-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
3-Methoxynaphthalene-1-carboxylicacid
1g
$ 1819.80

Alichem
3-Methoxynaphthalene-1-carboxylicacid
500mg
$ 1029.00

Alichem
3-Methoxynaphthalene-1-carboxylicacid
250mg
$ 720.80

Total 5 raw suppliers

Chemical Property of 3-Methoxynaphthalene-1-carboxylic acid

Chemical Property:

Melting Point:159 °C
Boiling Point:403.3±18.0 °C(Predicted)
PKA:3.51±0.10(Predicted)
PSA：46.53000
Density:1.263±0.06 g/cm3(Predicted)
LogP:2.54660
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:202.062994177
Heavy Atom Count:15
Complexity:239

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxynaphthalene-1-carboxylicacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC2=CC=CC=C2C(=C1)C(=O)O

Technology Process of 3-Methoxynaphthalene-1-carboxylic acid

There total 9 articles about 3-Methoxynaphthalene-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 147397-59-9
1-cyano-3-methoxynaphthalene

: 147397-60-2
3-methoxy-1-naphthoic acid

Guidance literature:: With sodium hydroxide; In ethanol; for 24h; Heating;
DOI:10.1021/ja00059a012

Reference yield:

: 5111-34-2
1-bromo-3-methoxy-naphthalene

: 147397-60-2
3-methoxy-1-naphthoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / dimethylformamide / 6 h / Heating

2: 95 percent / 2.5 M NaOH / ethanol / 24 h / Heating

With sodium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja00059a012

Reference yield:

: 5289-78-1
3-methoxy-1,8-naphthalic anhydride

: 147397-60-2
3-methoxy-1-naphthoic acid

: 36112-61-5
6-methoxy-1-naphthoic acid

Guidance literature:: 3-methoxy-1,8-naphthalic anhydride; With sodium hydroxide; In water; at 100 ℃; for 0.0166667h; microwave irradiation;

With mercury(II) diacetate; In water; at 180 ℃; for 0.25h; microwave irradiation;

With hydrogenchloride; In water; at 120 ℃; for 0.25h; Title compound not separated from byproducts; microwave irradiation;
DOI:10.1016/j.tet.2005.12.064