6-chloro-N,N-diisopropylnicotinaMide

Base Information

Chemical Name:6-chloro-N,N-diisopropylnicotinaMide
CAS No.:905273-87-2
Molecular Formula:C12H17ClN2O
Molecular Weight:240.72918
Hs Code.:
Mol file:905273-87-2.mol

Synonyms:6-chloro-N,N-diisopropylnicotinaMide;6-chloranyl-N,N-di(propan-2-yl)pyridine-3-carboxaMide;6-chloro-N,N-diisopropylpyridine-3-carboxamide

Suppliers and Price of 6-chloro-N,N-diisopropylnicotinaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
6-Chloro-N,N-diisopropylnicotinamide 95%
1g
$ 97.00

Matrix Scientific
6-Chloro-N,N-diisopropylnicotinamide 95%
5g
$ 296.00

Matrix Scientific
6-Chloro-N,N-diisopropylnicotinamide 95%
10g
$ 455.00

Crysdot
6-chloro-N,N-diisopropylnicotinamide 95+%
1g
$ 149.00

Crysdot
6-chloro-N,N-diisopropylnicotinamide 95+%
10g
$ 772.00

Crysdot
6-chloro-N,N-diisopropylnicotinamide 95+%
5g
$ 446.00

Chemenu
6-chloro-N,N-diisopropylnicotinamide 95%
5g
$ 421.00

Chemenu
6-chloro-N,N-diisopropylnicotinamide 95%
10g
$ 729.00

Ambeed
6-Chloro-N,N-diisopropylnicotinamide 95%
5g
$ 544.00

Ambeed
6-Chloro-N,N-diisopropylnicotinamide 95%
1g
$ 189.00

Total 2 raw suppliers

Chemical Property of 6-chloro-N,N-diisopropylnicotinaMide

Chemical Property:

PSA：33.20000
LogP:2.99400
Storage Temp.:Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

6-Chloro-N,N-diisopropylnicotinamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-chloro-N,N-diisopropylnicotinaMide

There total 2 articles about 6-chloro-N,N-diisopropylnicotinaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.35%

: 58757-38-3
6-Chloronicotinoyl chloride

: 108-18-9
diisopropylamine

: 905273-87-2
6-chloro-N,N-bis(propan-2-yl)pyridine-3-carboxamide

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 15h;

Reference yield:

: 5326-23-8
6-Chloro-3-pyridinecarboxylic acid

: 905273-87-2
6-chloro-N,N-bis(propan-2-yl)pyridine-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / toluene; N,N-dimethyl-formamide / 5 h / 85 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 10 °C

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2013.06.090

Reference yield: 86.8%

: 905273-87-2
6-chloro-N,N-bis(propan-2-yl)pyridine-3-carboxamide

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 905273-88-3
6-chloro-4-formyl-N,N-bis(propan-2-yl)pyridine-3-carboxamide

Guidance literature:: 6-chloro-N,N-bis(propan-2-yl)pyridine-3-carboxamide; With n-butyllithium; diisopropylamine; In diethyl ether; at -78 ℃; for 0.25h;

N,N-dimethyl-formamide; In diethyl ether; at -78 ℃; for 1h;