(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Base Information

Chemical Name:(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%
CAS No.:1091606-63-1
Molecular Formula:C19H21NO5S
Molecular Weight:375.445
Hs Code.:
Mol file:1091606-63-1.mol

Synonyms:(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Suppliers and Price of (4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%
1g
$ 283.00

Strem Chemicals
(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%
250mg
$ 94.00

Total 5 raw suppliers

Chemical Property of (4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Chemical Property:

Melting Point:152.5-153.4 °C
Boiling Point:477.2±55.0 °C(Predicted)
PKA:-14.89±0.60(Predicted)
PSA：81.29000
Density:1.281±0.06 g/cm3(Predicted)
LogP:4.99980
Sensitive.:air sensitive

Purity/Quality:

97% ^*data from raw suppliers

(4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

There total 9 articles about (4S,5R)-4,5-Diphenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1293372-43-6
(4S,5R)-4,5-diphenyl-[1,2,3]oxathiazolidine 2,2-dioxide

: 1091606-63-1
(4S,5R)-4,5-diphenyl-1,2,3-oxathiazolidine-3-carboxylic acid 1,1-dimethylethyl ester 2,2-dioxide

Guidance literature:: With dmap; In dichloromethane; at 25 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c0cc05289b

Reference yield: 84.7%

: (4S,5R)-4,5-diphenyl-1,2,3-oxathiazolidine-3-carboxylic acid 1,1-dimethylethyl ester 2-oxide

: 1091606-63-1
(4S,5R)-4,5-diphenyl-1,2,3-oxathiazolidine-3-carboxylic acid 1,1-dimethylethyl ester 2,2-dioxide

Guidance literature:: With ruthenium trichloride; sodium periodate; In dichloromethane; water; acetonitrile; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c0cc05289b

Reference yield:

: 23190-16-1
(1R,2S)-2-Amino-1,2-diphenylethanol

: 1091606-63-1
(4S,5R)-4,5-diphenyl-1,2,3-oxathiazolidine-3-carboxylic acid 1,1-dimethylethyl ester 2,2-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / tetrahydrofuran; water / 3 h / 0 - 25 °C / Inert atmosphere

2: thionyl chloride; triethylamine / dichloromethane / 1 h / -40 °C / Inert atmosphere

3: sodium periodate; ruthenium trichloride / dichloromethane; water; acetonitrile / 4 h / 0 °C / Inert atmosphere

With ruthenium trichloride; sodium periodate; thionyl chloride; sodium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1039/c0cc05289b