2-([(4-CHLOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID

Base Information

• Chemical Name: 2-([(4-CHLOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID
• CAS No.: 90410-27-8
• Molecular Formula: C9H10ClNO4S
• Molecular Weight: 263.702
• Hs Code.: 2935009090
• Mol file: 90410-27-8.mol

Synonyms:N-[(4-chlorophenyl)sulfonyl]-L-alanine

Chemical Property of 2-([(4-CHLOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID

Chemical Property:

• Vapor Pressure: 1.01E-08mmHg at 25°C
• Boiling Point: 445.6°C at 760 mmHg
• Flash Point: 223.3°C
• PSA: 91.85000
• Density: 1.465g/cm³
• LogP: 2.56310

Purity/Quality:

98%min ^*data from raw suppliers

2-{[(4-Chlorophenyl)sulfonyl]amino}propanoic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-([(4-CHLOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID

There total 2 articles about 2-([(4-CHLOROPHENYL)SULFONYL]AMINO)PROPANOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-chlorobenzenesulfonyl chloride (98-60-2) + rac-Ala-OH (302-72-7,25191-17-7,18875-37-1) → N-[(4-chlorophenyl)sulfonyl]alanine (90410-27-8)

Guidance literature:

With sodium hydroxide; In water; at 60 - 70 ℃; for 0.5h;

DOI:10.1002/jps.2600760213

Reference yield:

→ N-[(4-chlorophenyl)sulfonyl]alanine (90410-27-8)

Guidance literature:

Alanin + 4-Chlor-benzolsulfonylchlorid + wss. NaOH;

Reference yield: 89.0%

2-amino-N-phenyl-acetamide (555-48-6) + N-[(4-chlorophenyl)sulfonyl]alanine (90410-27-8) → 2-((4-chlorophenyl)sulfonamido)-N-(2-oxo-2-(phenylamino)ethyl)propanamide

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/d0nj04387g

upstream raw materials:

4-chlorobenzenesulfonyl chloride

rac-Ala-OH

Downstream raw materials:

N-[(4-chloro-phenyl)sulfonyl]alanyl chloride

4-chloro-N-(1-methyl-2-oxo-pentyl)-benzenesulfonamide

N₂-[(4-chloro-phenyl)sulfonyl]-N₁-methoxy-N₁-methyl-alaninamide

4-chloro-N-[1-(4,5-diethyl-1H-pyrazol-3-yl)ethyl]benzenesulfonamide

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