THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0

Base Information

• Chemical Name: THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0
• CAS No.: 173612-58-3
• Molecular Formula: C24 H24 Cl6 N6 O3 P4 S4
• Molecular Weight: 909.37
• Hs Code.: 29310099
• Mol file: 173612-58-3.mol

Synonyms:THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0;THIOPHOSPHORYL-PPMH-3 DENDRIMER GENERA

Chemical Property of THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0

Chemical Property:

• PSA: 242.09000
• LogP: 13.95370

Purity/Quality:

98% ^*data from raw suppliers

THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0 95.00% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0

There total 3 articles about THIOPHOSPHORYL-PMMH-3 DENDRIMER, GENERATION 1.0 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxybenzaldehyde sodium salt (22666-84-8) → tris(4-N'-dichloro(thio)phosphonyl)-(N'-methyldiazobenzene)monophosphate (173612-58-3)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₃S

With trichlorothiophosphine; 1: Substitution / 2: Condensation;

DOI:10.1021/ac0003854

Reference yield:

dichloro(1-methylhydrazido)thiophosphane (61609-05-0) + O,O,O-tris(4-formylphenyl) phosphorothioate (159213-45-3) → tris(4-N'-dichloro(thio)phosphonyl)-(N'-methyldiazobenzene)monophosphate (173612-58-3)

Guidance literature:

With 4 A molecular sieve; In chloroform; at 25 ℃; Yield given;

Reference yield:

girard's reagent T (123-46-6) + O,O,O-tris(4-formylphenyl) phosphorothioate (159213-45-3) → tris(4-N'-dichloro(thio)phosphonyl)-(N'-methyldiazobenzene)monophosphate (173612-58-3)

Guidance literature:

upstream raw materials:

dichloro(1-methylhydrazido)thiophosphane

O,O,O-tris(4-formylphenyl) phosphorothioate

4-hydroxybenzaldehyde sodium salt

girard's reagent T

Downstream raw materials:

G'1

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