11-Nor-9-carboxy-thc

Base Information

Chemical Name:11-Nor-9-carboxy-thc
CAS No.:64280-14-4
Molecular Formula:C₂₁H₂₈O₄
Molecular Weight:344.451
Hs Code.:
DSSTox Substance ID:DTXSID8074788
Nikkaji Number:J360.962F
Wikipedia:11-Nor-9-carboxy-THC
Wikidata:Q4547226

Synonyms:(6aR-trans)-isomer of 11-nor-delta(9)-tetrahydrocannabinol-9-carboxylic acid;11-nor-9-carboxy-delta(9)-tetrahydrocannabinol;11-nor-9-carboxy-delta-9-tetrahydrocannabinol;11-nor-9-carboxy-THC;11-nor-delta(9)-tetrahydrocannabinol-9-carboxylic acid;delta(1)-tetrahydrocannabinol-7-oic acid;delta(9)-tetrahydrocannabinol-11-oic-acid;delta-9-11-carboxytetrahydrocannabinol;hexadeutero-11-nor-delta(9)-tetrahydrocannabinol-9-carboxylic acid;tetrahydrocannabinol-7-oic acid;THC-11-oic acid

Suppliers and Price of 11-Nor-9-carboxy-thc

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DL-11-NOR-9-CARBOXY-DELTA-9-THC 95.00%
5MG
$ 501.33

Total 2 raw suppliers

Chemical Property of 11-Nor-9-carboxy-thc

Chemical Property:

Vapor Pressure:1.62E-09mmHg at 25°C
Boiling Point:466.9°Cat760mmHg
Flash Point:158.1°C
PSA：66.76000
Density:1.14g/cm³
LogP:4.80050
XLogP3:6.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:344.19875937
Heavy Atom Count:25
Complexity:524

Purity/Quality:

99% ^*data from raw suppliers

DL-11-NOR-9-CARBOXY-DELTA-9-THC 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC1=CC(=C2C3C=C(CCC3C(OC2=C1)(C)C)C(=O)O)O

Technology Process of 11-Nor-9-carboxy-thc

There total 12 articles about 11-Nor-9-carboxy-thc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 124-38-9,18923-20-1
carbon dioxide

: 949595-94-2
C₃₅H₅₂N₂O₄S

: 36557-05-8,56354-06-4,64280-14-4,104874-50-2,114028-39-6,122797-75-5
11-nor-9-carboxt-Δ-9-tetrahydrocannabinol

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; 1.) -78 deg C to 0 deg C, 30 min, 2.) 3 min;
DOI:10.1021/jo970969e

Reference yield:

: 138285-38-8
(-)-11-nor-9-carboxy-Δ⁹-tetrahydrocannabinol tert-butyldimethylsilyl ether

: 36557-05-8,56354-06-4,64280-14-4,104874-50-2,114028-39-6,122797-75-5
11-nor-9-carboxt-Δ-9-tetrahydrocannabinol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; Ambient temperature;
DOI:10.1055/s-1991-26590

Reference yield:

: 52195-11-6
(-)-9-Nor-9-oxohexahydrocannabinol

: 36557-05-8,56354-06-4,64280-14-4,104874-50-2,114028-39-6,122797-75-5
11-nor-9-carboxt-Δ-9-tetrahydrocannabinol

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / 0.08 h / 27 °C

2: 54 percent / n-BuLi, TMEDA / hexane / 1.) -78 deg C to 0 deg C, 30 min, 2.) 3 min

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In ethanol; hexane;
DOI:10.1021/jo970969e