Technology Process of Magnesium, dioctyl-
There total 2 articles about Magnesium, dioctyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
magnesium hydride;
zirconium(IV) iodide;
In
tetrahydrofuran;
for 2h;
Product distribution;
Heating;
diff. catalysts and without catalyst, standard pressure;
- Guidance literature:
-
In
tetrahydrofuran; n-heptane;
a soln. of SnCl4 (18 mmol) in heptane was added dropwise within 10 min to a soln. of (C8H17)2Mg (44 mmol) in THF with stirring (pptn.); the mixt. was refluxed for 3 1/3 h, then treated with H2O and 10% HCl;; the org. layer was separated and dried with CaCl2, the solvents were distilled off in vac., the residue was istilled in high vac.; 99.1% purity (asdetermined by gas chromy.); identified by mass spectrometry; elem. anal.;;