methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate

Base Information

Chemical Name:methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate
CAS No.:1131872-40-6
Molecular Formula:C₁₅H₂₁NO₅
Molecular Weight:295.335
Hs Code.:
Mol file:1131872-40-6.mol

Synonyms:methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate

Suppliers and Price of methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

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Technology Process of methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate

There total 2 articles about methyl 2-(tert-butoxycarbonylamino)-2-(4-hydroxy-2-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67-56-1
methanol

: 1131872-37-1
2-amino-2-(4-hydroxy-2-methylphenyl)acetic acid hydrochloride

: 24424-99-5
di-tert-butyl dicarbonate

: 1131872-40-6
tert-butoxycarbonylamino-(4-hydroxy-2-methylphenyl)acetic acid methyl ester

Guidance literature:: methanol; 2-amino-2-(4-hydroxy-2-methylphenyl)acetic acid hydrochloride; With thionyl chloride; at 0 - 20 ℃;

di-tert-butyl dicarbonate; With N-ethyl-N,N-diisopropylamine; In methanol; at 0 - 20 ℃; for 36h;

Reference yield:

: 1131872-40-6
tert-butoxycarbonylamino-(4-hydroxy-2-methylphenyl)acetic acid methyl ester

Guidance literature:

Reference yield: 94.0%

: 1131872-40-6
tert-butoxycarbonylamino-(4-hydroxy-2-methylphenyl)acetic acid methyl ester

: 1147391-58-9
tert-butyl 2-hydroxy-1-(4-hydroxy-2-methylphenyl)ethylcarbamate

Guidance literature:: tert-butoxycarbonylamino-(4-hydroxy-2-methylphenyl)acetic acid methyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; pH=2;