Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI)

Base Information

• Chemical Name: Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI)
• CAS No.: 191725-82-3
• Molecular Formula: C₈H₉NO₂
• Molecular Weight: 151.165
• Hs Code.: 2933399090
• Mol file: 191725-82-3.mol

Synonyms:Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI);3-Acetyl-4-Methoxy pyridine;1-(4-Methoxypyridin-3-yl)ethanone;1-(4-Methoxy-3-pyridinyl)ethanone;1-(4-Methoxy-3-pyridyl)ethanone;1-(4-methoxypyridin-3-yl)ethan-1-one

Chemical Property of Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI)

Chemical Property:

• Boiling Point: 264.2±20.0 °C(Predicted)
• PKA: 4.75±0.18(Predicted)
• PSA: 39.19000
• Density: 1.093±0.06 g/cm3(Predicted)
• LogP: 1.29280

Purity/Quality:

99%, ^*data from raw suppliers

1-(4-Methoxypyridin-3-yl)ethanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI)

There total 3 articles about Ethanone, 1-(4-methoxy-3-pyridinyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-(4-chloropyridin-3-yl)ethanone (116922-73-7) → 1-(4-methoxypyridin-3-yl)ethanone (191725-82-3)

Guidance literature:

In methanol; water; sodium methylate;

Reference yield: 76.0%

1-(4-chloropyridin-3-yl)ethanone hydrochloride (1807467-70-4) + sodium methylate (124-41-4) → 1-(4-methoxypyridin-3-yl)ethanone (191725-82-3)

Guidance literature:

In methanol; for 1h; Inert atmosphere; Reflux;

DOI:10.1016/j.bmc.2015.07.056

Reference yield:

rac-4-chloro-3-(1-hydroxyethyl)pyridine (116922-69-1) → 1-(4-methoxypyridin-3-yl)ethanone (191725-82-3)

Guidance literature:

Multi-step reaction with 2 steps

1: chromium(VI) oxide

2: methanol / 1 h / Reflux; Inert atmosphere

With chromium(VI) oxide; In methanol;

upstream raw materials:

1-(4-chloropyridin-3-yl)ethanone

1-(4-chloropyridin-3-yl)ethanone hydrochloride

sodium methylate

rac-4-chloro-3-(1-hydroxyethyl)pyridine

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