ethyl 4-butyrylbenzoate

Base Information

Chemical Name:ethyl 4-butyrylbenzoate
CAS No.:1383800-57-4
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:
Mol file:1383800-57-4.mol

Synonyms:ethyl 4-butyrylbenzoate

Suppliers and Price of ethyl 4-butyrylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
Ethyl 4-butyrylbenzoate 95%
2.500g
$ 1403.00

Crysdot
Ethyl4-butyrylbenzoate 95+%
1g
$ 428.00

A1 Biochem Labs
Ethyl4-butyrylbenzoate 95%
2.5 g
$ 850.00

Total 2 raw suppliers

Chemical Property of ethyl 4-butyrylbenzoate

Chemical Property:

PSA：43.37000
LogP:2.84610

Purity/Quality:

99% ^*data from raw suppliers

Ethyl 4-butyrylbenzoate 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 4-butyrylbenzoate

There total 3 articles about ethyl 4-butyrylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 5798-75-4
Ethyl 4-bromobenzoate

: 123-72-8
butyraldehyde

: 1383800-57-4
ethyl 4-butyrylbenzoate

Guidance literature:: With nickel(II) iodide; potassium phosphate; tetrakis(tetrabutylammonium)decatungstate(VI); 4,4'-di-tert-butyl-2,2'-bipyridine; In acetonitrile; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.0c01121

Reference yield:

: 1355533-73-1
ethyl 4-(1-hydroxybutyl)benzoate

: 1383800-57-4
ethyl 4-butyrylbenzoate

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 0 - 20 ℃; for 3h;

Reference yield:

: 51934-41-9
4-iodobenzoic acid ethyl ester

: 1383800-57-4
ethyl 4-butyrylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: TurboGrignard / tetrahydrofuran / 0.67 h / -40 °C

1.2: 3 h / -40 - 20 °C

2.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 3 h / 0 - 20 °C

With TurboGrignard; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;