tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate

Base Information

• Chemical Name: tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate
• CAS No.: 360792-43-4
• Molecular Formula: C19H30BNO4
• Molecular Weight: 347.262
• Mol file: 360792-43-4.mol

Synonyms:tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate

Chemical Property of tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate

Chemical Property:

• PSA: 56.79000
• LogP: 3.44390

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate

There total 13 articles about tert-butyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

t-butyl 2-(4-bromophenyl)ethylcarbamate (120157-97-3) + bis(pinacol)diborane (73183-34-3) → tert-butyl N-[2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethyl]carbamate (360792-43-4)

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 80 ℃; for 18h;

Reference yield: 100.0%

tert-butyl {2,2,2-trifluoro-N-[2-(4-(boronic acid)phenyl)ethyl]acetylamino}formate, pinacol ester (360792-42-3) → tert-butyl N-[2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethyl]carbamate (360792-43-4)

Guidance literature:

With sodium carbonate; In propan-1-ol; diethyl ether; for 2h;

Reference yield: 80.0%

bis(pinacol)diborane (73183-34-3) + tert-butyl (4-((diethoxyphosphoryl)oxy)phenethyl)carbamate (245321-43-1) → tert-butyl N-[2-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethyl]carbamate (360792-43-4)

Guidance literature:

With 10H-phenothiazine; caesium carbonate; In acetonitrile; for 48h; Irradiation; Sealed tube; Inert atmosphere;

DOI:10.1021/jacs.9b12519

upstream raw materials:

t-butyl 2-(4-bromophenyl)ethylcarbamate

bis(pinacol)diborane

tert-butyl {2,2,2-trifluoro-N-[2-(4-(boronic acid)phenyl)ethyl]acetylamino}formate, pinacol ester

di-tert-butyl dicarbonate

Downstream raw materials:

2-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)ethan-1-amine

C₂₅H₄₀BN₃O₆

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