1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester

Base Information

• Chemical Name: 1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester
• CAS No.: 853685-78-6
• Molecular Formula: C₉H₈N₂O₂
• Molecular Weight: 176.175
• Hs Code.: 2933990090
• Mol file: 853685-78-6.mol

Synonyms:1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester;methyl 1H-pyrrolo[3,2-c]pyridine-2-carboxylate

Chemical Property of 1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester

Chemical Property:

• PSA: 54.98000
• LogP: 1.34950

Purity/Quality:

99%, ^*data from raw suppliers

MethylPyrrolo[3,2-C]pyridine-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester

There total 5 articles about 1H-Pyrrolo[3,2-c]pyridine-2-carboxylic acid, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

methanol (67-56-1) + 1H-pyrrolo[3,2-c]pyridine-2-carbaldehyde (630395-95-8) → 1H-pyrrolo[3,2-c]pyridine-2-carboxylic acid methyl ester (853685-78-6)

Guidance literature:

With sodium cyanide; manganese(IV) oxide; at 0 ℃; for 5h; Inert atmosphere;

Reference yield: 48.0%

methyl (2Z)-3-(4-bromo(3-pyridyl))-2-[(phenylmethoxy)carbonylamino]prop-2-enoate (1196699-67-8) → 1H-pyrrolo[3,2-c]pyridine-2-carboxylic acid methyl ester (853685-78-6)

Guidance literature:

With potassium carbonate; L-proline; copper(l) iodide; In 1,4-dioxane; Inert atmosphere;

Reference yield: 46.0%

methanol (67-56-1) + ethyl 1-tosyl-1H-pyrrolo[3,2-c]pyridine-2-carboxylate (1383252-76-3) → 1H-pyrrolo[3,2-c]pyridine-2-carboxylic acid methyl ester (853685-78-6)

Guidance literature:

With caesium carbonate; In tetrahydrofuran; at 15 ℃; for 12h;

upstream raw materials:

methanol

1H-pyrrolo[3,2-c]pyridine-2-carbaldehyde

methyl (2Z)-3-(4-bromo(3-pyridyl))-2-[(phenylmethoxy)carbonylamino]prop-2-enoate

5-azaindole

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