9-Methoxyphenanthridine

Base Information

• Chemical Name: 9-Methoxyphenanthridine
• CAS No.: 41001-28-9
• Molecular Formula: C₁₄H₁₁NO
• Molecular Weight: 209.247
• DSSTox Substance ID: DTXSID101313657
• Nikkaji Number: J89.391I
• Mol file: 41001-28-9.mol

Synonyms:9-methoxyphenanthridine;9-methoxy-phenanthridine;41001-28-9;DTXSID101313657

Chemical Property of 9-Methoxyphenanthridine

Chemical Property:

• XLogP3: 3.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 209.084063974
• Heavy Atom Count: 16
• Complexity: 243

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC2=C(C=C1)C=NC3=CC=CC=C32

Technology Process of 9-Methoxyphenanthridine

There total 20 articles about 9-Methoxyphenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

N-(4-methoxybenzylidene)aniline (1613-96-3) → 9-methoxyphenanthridine (41001-28-9)

Guidance literature:

With tert-butyl alcohol; at 45 ℃; for 2h; UV-irradiation; Green chemistry;

DOI:10.1016/j.tetlet.2020.152734

Reference yield: 68.0%

acrylonitrile (107-13-1,25014-41-9) + 3'-methoxy-[1,1'-biphenyl]-2-amine (38089-02-0) → 9-methoxyphenanthridine (41001-28-9)

Guidance literature:

With silver hexafluoroantimonate; [RhCl₂(p-cymene)]2; mesitylenecarboxylic acid; copper(II) acetate monohydrate; In tetrahydrofuran; at 80 ℃; for 48h; Glovebox; Inert atmosphere;

DOI:10.1039/c9cc05717j

Reference yield: 51.0%

N-((5-methoxy-[1,1′-biphenyl]-2-yl)methyl)-4-methylbenzenesulfonamide → 9-methoxyphenanthridine (41001-28-9)

Guidance literature:

With [bis(acetoxy)iodo]benzene; iodine; In nitromethane; at 20 ℃; for 3h; Irradiation;

DOI:10.1021/acs.joc.0c01390

upstream raw materials:

p-methoxybenzylidene-phenylamine

2-(3-methoxyphenyl)benzyl bromide

C₁₄H₁₃N₃O

3'-methoxy-[1,1′]-biphenyl-2-carbaldehyde

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