3-Methoxymethoxy-2-tributylstannylpyridine

Base Information

Chemical Name:3-Methoxymethoxy-2-tributylstannylpyridine
CAS No.:405137-20-4
Molecular Formula:C₁₉H₃₅NO₂Sn
Molecular Weight:428.202
Hs Code.:
DSSTox Substance ID:DTXSID80478586
Mol file:405137-20-4.mol

Synonyms:3-Methoxymethoxy-2-tributylstannylpyridine;405137-20-4;tributyl-[3-(methoxymethoxy)pyridin-2-yl]stannane;3-(methoxymethoxy)-2-(tributylstannyl)pyridine;Pyridine, 3-(methoxymethoxy)-2-(tributylstannyl)-;DTXSID80478586;AKOS015843262;GS-6567;CS-0081700;FT-0685538;F11344;A914037;J-512793

Suppliers and Price of 3-Methoxymethoxy-2-tributylstannylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
3-Methoxymethoxy-2-tributylstannylpyridine
5g
$ 4945.00

Matrix Scientific
3-Methoxymethoxy-2-tributylstannylpyridine
1g
$ 2540.00

Total 12 raw suppliers

Chemical Property of 3-Methoxymethoxy-2-tributylstannylpyridine

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:445.9°C at 760 mmHg
PKA:4.37±0.10(Predicted)
Flash Point:223.472°C
PSA：31.35000
LogP:4.81010
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:13
Exact Mass:429.168982
Heavy Atom Count:23
Complexity:267

Purity/Quality:

97% ^*data from raw suppliers

3-Methoxymethoxy-2-tributylstannylpyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=C(C=CC=N1)OCOC

Technology Process of 3-Methoxymethoxy-2-tributylstannylpyridine

There total 2 articles about 3-Methoxymethoxy-2-tributylstannylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1461-22-9
tri-n-butylstannyl chloride

: 87905-88-2
2-iodo-3-(methoxymethoxy)pyridine

: 405137-20-4
3-(methoxymethoxy)-2-(tributylstannyl)pyridine

Guidance literature:: 2-iodo-3-(methoxymethoxy)pyridine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

tri-n-butylstannyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2.16667h;

Reference yield:

: 40263-57-8
2-iodo-3-hydroxypyridine

: 405137-20-4
3-(methoxymethoxy)-2-(tributylstannyl)pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C

1.2: 1.17 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.2: 2.17 h / -78 - 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; mineral oil;

Reference yield:

: 405137-20-4
3-(methoxymethoxy)-2-(tributylstannyl)pyridine

: 5'-bromo-1'-(2-fluorophenyl)-3-(methoxymethoxy)-2'-methyl-[2,3'-bipyridin]-6'(1'H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 7 h / 150 °C / Microwave irradiation

2: N-Bromosuccinimide / acetonitrile / 12 h / 20 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; acetonitrile;