4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole

Base Information

Chemical Name:4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole
CAS No.:1314801-35-8
Molecular Formula:C₂₂H₃₄Br₂N₂O₃
Molecular Weight:534.332
Hs Code.:
Mol file:1314801-35-8.mol

Synonyms:4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole;4,7-Dibromo-5,6-dihydroperoxybenzo[c][1,2,5]oxadiazole

Suppliers and Price of 4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
4,7-Dibromo-5,6-dihydroperoxybenzo[c][1,2,5]oxadiazole 95+%
1g
$ 1488.00

Chemenu
4,7-dibromo-5,6-dihydroperoxybenzo[c][1,2,5]oxadiazole 95%
1g
$ 1403.00

Total 9 raw suppliers

Chemical Property of 4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole

Chemical Property:

PSA：97.84000
LogP:2.45140

Purity/Quality:

98% purity ^*data from raw suppliers

4,7-Dibromo-5,6-dihydroperoxybenzo[c][1,2,5]oxadiazole 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole

There total 5 articles about 4,7-DibroMo-5,6-bis(oxtyloxy)benzo-2,1,3-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1314801-34-7
5,6-bis(octyloxy)benzo[c][1,2,5]oxadiazole

: 1314801-35-8
4,7-dibromo-5,6-bis(octyloxy)benzo[c][1,2,5]oxadiazole

Guidance literature:: With bromine; acetic acid; In dichloromethane; at 20 ℃; for 72h; Darkness;
DOI:10.1039/c1cc12040a

Reference yield:

: 4956-41-6
1,2-dioctyloxybenzene

: 1314801-35-8
4,7-dibromo-5,6-bis(octyloxy)benzo[c][1,2,5]oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid; acetic acid / dichloromethane / 41 h / 10 - 20 °C

2.1: sodium azide; tetrabutylammomium bromide / toluene / Reflux

2.2: 24 h / Reflux

3.1: bromine; acetic acid / dichloromethane / 72 h / 20 °C / Darkness

With sodium azide; tetrabutylammomium bromide; bromine; nitric acid; acetic acid; In dichloromethane; toluene;
DOI:10.1039/c1cc12040a

Reference yield:

: 156777-91-2
1,2-bis(octyloxy)-4,5-dinitrobenzene

: 1314801-35-8
4,7-dibromo-5,6-bis(octyloxy)benzo[c][1,2,5]oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide; tetrabutylammomium bromide / toluene / Reflux

1.2: 24 h / Reflux

2.1: bromine; acetic acid / dichloromethane / 72 h / 20 °C / Darkness

With sodium azide; tetrabutylammomium bromide; bromine; acetic acid; In dichloromethane; toluene;
DOI:10.1039/c1cc12040a