ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate

Base Information

Chemical Name:ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate
CAS No.:104036-19-3
Molecular Formula:C10H18O3
Molecular Weight:186.251
Hs Code.:
Mol file:104036-19-3.mol

Synonyms:ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate

Suppliers and Price of ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
Ethyl4-hydroxy-1-methylcyclohexanecarboxylate 97%
0.5g
$ 293.33

Total 5 raw suppliers

Chemical Property of ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate

Chemical Property:

PSA：46.53000
LogP:1.49070

Purity/Quality:

97% ^*data from raw suppliers

Ethyl4-hydroxy-1-methylcyclohexanecarboxylate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate

There total 6 articles about ethyl 4-hydroxy-1-Methylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 147905-77-9
ethyl 1-methyl-4-oxo-1-cyclohexanecarboxylate

: 104036-19-3
ethyl 4-hydroxy-1-methylcyclohexane-1-carboxylate

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 ℃; for 1.5h;

Reference yield: 63.0%

: 1124173-50-7
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

: 104036-19-3
ethyl 4-hydroxy-1-methylcyclohexane-1-carboxylate

Guidance literature:: ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 35h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 1489-97-0
ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate

: 104036-19-3
ethyl 4-hydroxy-1-methylcyclohexane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / -78 °C

2.1: hydrogenchloride / water; acetone / 48 h / 20 °C

3.1: sodium tetrahydroborate; methanol / 1.5 h / 0 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; lithium diisopropyl amide; In tetrahydrofuran; water; acetone;