ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

Base Information

Chemical Name:ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate
CAS No.:1124173-50-7
Molecular Formula:C₁₆H₃₂O₃Si
Molecular Weight:300.514
Hs Code.:

Synonyms:ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

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Chemical Property of ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

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Technology Process of ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

There total 3 articles about ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 676560-15-9
Ethyl (cis/trans)-4-<(tert-butyldimethylsilyl)oxy>cyclohexanecarboxylate

: 74-88-4
methyl iodide

: 1124173-50-7
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

Guidance literature:: Ethyl (cis/trans)-4-<(tert-butyldimethylsilyl)oxy>cyclohexanecarboxylate; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 2.33h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃;

Reference yield:

: 3618-04-0,75877-66-6,17159-80-7
4-hydroxycyclohexyl carboxylic acid ethyl ester

: 1124173-50-7
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 3 h / -78 - 20 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1124173-50-7
ethyl 4-{[tert-butyl(dimethyl)silyl]oxy}-1-methylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

2.2: 3 h / -78 - 20 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;