4-Fluorobenzene-1,3-dioyl dichloride

Base Information

• Chemical Name: 4-Fluorobenzene-1,3-dioyl dichloride
• CAS No.: 327-94-6
• Molecular Formula: C₈H₃Cl₂FO₂
• Molecular Weight: 221.015
• Mol file: 327-94-6.mol

Synonyms:4-Fluorobenzene-1,3-dioyl dichloride;4-Fluoro-1,3-benzenedicarbonyl dichloride;4-Fluoroisophthaloyl chloride;4-Fluoroisophthaloyl dichloride

Chemical Property of 4-Fluorobenzene-1,3-dioyl dichloride

Chemical Property:

• Boiling Point: 262℃
• Flash Point: 112℃
• PSA: 34.14000
• Density: 1.509
• LogP: 2.58370

Purity/Quality:

97% ^*data from raw suppliers

4-Fluorobenzene-1,3-dioyldichloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Fluorobenzene-1,3-dioyl dichloride

There total 2 articles about 4-Fluorobenzene-1,3-dioyl dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-fluorobenzene-1,3-dioic acid (327-95-7) → 4-fluoro-isophthaloyl chloride (327-94-6)

Guidance literature:

With thionyl chloride;

DOI:10.1021/ja01252a016

Reference yield:

2,4-dimethylfluorobenzene (452-65-3) → 4-fluoro-isophthaloyl chloride (327-94-6)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous potassium permanganate

2: thionyl chloride

With potassium permanganate; thionyl chloride;

DOI:10.1021/ja01252a016

Reference yield:

3-diethylamino-propan-1-ol (622-93-5) + 4-fluoro-isophthaloyl chloride (327-94-6) → 4-fluoro-isophthalic acid bis-(3-diethylamino-propylester); dihydrochloride

Guidance literature:

With benzene;

DOI:10.1021/ja01252a016

upstream raw materials:

4-fluorobenzene-1,3-dioic acid

2,4-dimethylfluorobenzene

Downstream raw materials:

4-fluoro-isophthalic acid bis-(2-dipropylamino-ethyl ester); dihydrochloride

4-fluoro-isophthalic acid bis-(3-dipropylamino-propylester); dihydrochloride

4-fluoro-isophthalic acid bis-(2-dibutylamino-ethyl ester); dihydrochloride

4-fluoro-isophthalic acid bis-(3-dibutylamino-propylester); dihydrochloride

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