3,4-dichlorobenzenebutanamine

Base Information

Chemical Name:3,4-dichlorobenzenebutanamine
CAS No.:732189-89-8
Molecular Formula:C₁₀H₁₃Cl₂N
Molecular Weight:218.126
Hs Code.:

Synonyms:3,4-dichlorobenzenebutanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-dichlorobenzenebutanamine

Chemical Property:

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Technology Process of 3,4-dichlorobenzenebutanamine

There total 9 articles about 3,4-dichlorobenzenebutanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1429204-39-6
(E)-4-(4-azidobut-1-enyl)-1 ,2-dichlorobenzene

: 732189-89-8
4-(3,4-dichlorophenyl)butan-1-amine

Guidance literature:: With platinum(IV) oxide; hydrogen; In ethyl acetate; for 1.5h; under 760.051 Torr;

Reference yield:

: 7312-27-8
3,4-Dichlorocinnamic acid

: 732189-89-8
4-(3,4-dichlorophenyl)butan-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C

2: BH₃

3: (i) MeSO₂Cl, Py, (ii) /BRN= 4652394/

4: BH₃

With borane; hydrogen; palladium on activated charcoal;
DOI:10.1021/jm00260a003

Reference yield:

: 1429204-37-4
(E)-tert-butyl-(4-(3,4-dichlorophenyl)but-3-enyloxy)dimethylsilane

: 732189-89-8
4-(3,4-dichlorophenyl)butan-1-amine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C

2: triethylamine / dichloromethane / 0.75 h / 0 °C

3: sodium azide / N,N-dimethyl-formamide / 16 h / 20 °C

4: platinum(IV) oxide; hydrogen / ethyl acetate / 1.5 h / 760.05 Torr

With platinum(IV) oxide; sodium azide; tetrabutyl ammonium fluoride; hydrogen; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;