2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL

Base Information

Chemical Name:2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL
CAS No.:948916-00-5
Molecular Formula:C14H24N14O5
Molecular Weight:468.437
Hs Code.:
Mol file:948916-00-5.mol

Synonyms:2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL

Chemical Property:

PSA：316.20000
LogP:-1.25096

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Technology Process of 2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL

There total 2 articles about 2-[(2-AMINOETHYL)AMINO]-4,6-DIAZIDO-2,4,5,6-TETRADEOXY-3-O-(2,6-DIAZIDO-2,6-DIDEOXY-D-GLUCOPYRANOSYL)-D-MYO-INOSITOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 107-15-3,85404-18-8
ethylenediamine

: 182554-04-7
1,3,2′,6′-tetraazido-6,3′,4′-tri-O-acetylneamine

: 948916-00-5
epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine

Guidance literature:: trifluoromethylsulfonic anhydride; 1,3,2′,6′-tetraazido-6,3′,4′-tri-O-acetylneamine; In pyridine; dichloromethane; at 20 ℃; for 1.5h;

ethylenediamine; In tetrahydrofuran; at 20 ℃; for 24h; Further stages.;
DOI:10.1016/j.tet.2007.06.002

Reference yield:

: C₁₉H₂₃F₃N₁₂O₁₁S

: 107-15-3,85404-18-8
ethylenediamine

: 948916-00-5
epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine

Guidance literature:: at 20 ℃;
DOI:10.1016/j.bmcl.2009.03.021

Reference yield: 91.0%

: 948916-00-5
epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine

: 146426-54-2
4’-carboxylic acid-3’-azido-3’-deoxythymidine

: 948916-05-0
C₂₄H₃₃N₁₉O₉

Guidance literature:: epi-5-(2-aminoethyl)-amino-1,3,2',6'-tetraazido neamine; 4’-carboxylic acid-3’-azido-3’-deoxythymidine; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

With potassium carbonate; In methanol; at 20 ℃; for 2h; Further stages.;
DOI:10.1016/j.tet.2007.06.002