4-BroMo-2-Methyl-1,3-benzoxazole

Base Information

Chemical Name:4-BroMo-2-Methyl-1,3-benzoxazole
CAS No.:217326-69-7
Molecular Formula:C8H6BrNO
Molecular Weight:212.04334
Hs Code.:
Mol file:217326-69-7.mol

Synonyms:4-BroMo-2-Methyl-1,3-benzoxazole;4-bromo-2-methylbenzo[d]oxazole;4-bromo-2-methylBenzoxazole

Suppliers and Price of 4-BroMo-2-Methyl-1,3-benzoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-Bromo-2-methyl-1,3-benzoxazole
100mg
$ 220.00

Crysdot
4-Bromo-2-methylbenzo[d]oxazole 95+%
1g
$ 527.00

Chemcia Scientific
4-Bromo-2-methyl-benzooxazole 95%
2.5 G
$ 1100.00

Alichem
4-Bromo-2-methylbenzo[d]oxazole
1g
$ 10423.30

AK Scientific
4-Bromo-2-methyl-1,3-benzoxazole
250mg
$ 371.00

Activate Scientific
4-Bromo-2-methylbenzo[d]oxazole 97%
250 mg
$ 467.00

Total 5 raw suppliers

Chemical Property of 4-BroMo-2-Methyl-1,3-benzoxazole

Chemical Property:

Boiling Point:264.8±13.0 °C(Predicted)
PKA:-1.31±0.30(Predicted)
Density:1.606±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

4-Bromo-2-methyl-1,3-benzoxazole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-BroMo-2-Methyl-1,3-benzoxazole

There total 4 articles about 4-BroMo-2-Methyl-1,3-benzoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 614-76-6
N-acetyl-2-bromoaniline

: 217326-69-7
4-bromo-2-methylbenzo[d]oxazole

Guidance literature:: With dipotassium peroxodisulfate; trifluorormethanesulfonic acid; palladium diacetate; acetic acid; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Sealed tube;
DOI:10.1039/c7ob02566a

Reference yield:

: 116435-77-9
2-amino-3-bromophenol

: 78-39-7
Triethyl orthoacetate

: 217326-69-7
4-bromo-2-methylbenzo[d]oxazole

Guidance literature:: at 120 ℃; for 2h; Inert atmosphere;

Reference yield:

: 615-36-1
2-bromoaniline

: 217326-69-7
4-bromo-2-methylbenzo[d]oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: acetic acid; palladium diacetate; trifluorormethanesulfonic acid; dipotassium peroxodisulfate / N,N-dimethyl-formamide / 24 h / 100 °C / Sealed tube

With dipotassium peroxodisulfate; trifluorormethanesulfonic acid; palladium diacetate; acetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c7ob02566a