Technology Process of 4-BroMo-2-Methyl-1,3-benzoxazole
There total 4 articles about 4-BroMo-2-Methyl-1,3-benzoxazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dipotassium peroxodisulfate; trifluorormethanesulfonic acid; palladium diacetate; acetic acid;
In
N,N-dimethyl-formamide;
at 100 ℃;
for 24h;
Sealed tube;
DOI:10.1039/c7ob02566a
- Guidance literature:
-
at 120 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 20 °C
2: acetic acid; palladium diacetate; trifluorormethanesulfonic acid; dipotassium peroxodisulfate / N,N-dimethyl-formamide / 24 h / 100 °C / Sealed tube
With
dipotassium peroxodisulfate; trifluorormethanesulfonic acid; palladium diacetate; acetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c7ob02566a