Methyl 2-cyano-4-fluoro-5-methoxybenzoate

Base Information

• Chemical Name: Methyl 2-cyano-4-fluoro-5-methoxybenzoate
• CAS No.: 1007455-23-3
• Molecular Formula: C10H8FNO3
• Molecular Weight: 209.177
• Hs Code.: 2916310090
• Mol file: 1007455-23-3.mol

Synonyms:Methyl 2-cyano-4-fluoro-5-methoxybenzoate;2-Cyano-4-fluoro-5-methoxy-benzoic acid methyl ester

Chemical Property of Methyl 2-cyano-4-fluoro-5-methoxybenzoate

Chemical Property:

• PSA: 59.32000
• LogP: 1.49258

Purity/Quality:

98%min ^*data from raw suppliers

Methyl 2-cyano-4-fluoro-5-methoxybenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 2-cyano-4-fluoro-5-methoxybenzoate

There total 6 articles about Methyl 2-cyano-4-fluoro-5-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

methyl 2-bromo-4-fluoro-5-methoxybenzoate (1007455-22-2) + copper(l) cyanide → methyl 2-cyano-4-fluoro-5-methoxybenzoate (1007455-23-3)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 4h;

Reference yield: 68.0%

methyl 2-bromo-4-fluoro-5-methoxybenzoate (1007455-22-2) + copper(I) cyanide (544-92-3) → methyl 2-cyano-4-fluoro-5-methoxybenzoate (1007455-23-3)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 3h;

Reference yield: 68.0%

copper(I) cyanide + methyl 2-bromo-4-fluoro-5-methoxybenzoate (1007455-22-2) → methyl 2-cyano-4-fluoro-5-methoxybenzoate (1007455-23-3)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 3h;

DOI:10.1016/j.tetlet.2008.12.099

upstream raw materials:

methyl 2-bromo-4-fluoro-5-methoxybenzoate

copper(I) cyanide

2-bromo-4-fluoro-5-methoxy-benzoic acid

4?fluoro-3-methoxybenzoic acid

Downstream raw materials:

5-fluoro-6-methoxyisoindolin-1-one

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