2-Deoxy-D-arabino-hexonic acid methyl ester

Base Information

• Chemical Name: 2-Deoxy-D-arabino-hexonic acid methyl ester
• CAS No.: 27963-68-4
• Molecular Formula: C₇H₁₄O₆
• Molecular Weight: 194.185
• Mol file: 27963-68-4.mol

Synonyms:2-Deoxy-D-arabino-hexonic acid methyl ester

Chemical Property of 2-Deoxy-D-arabino-hexonic acid methyl ester

Chemical Property:

• PSA: 107.22000
• LogP: -2.37550

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Deoxy-D-arabino-hexonic acid methyl ester

There total 4 articles about 2-Deoxy-D-arabino-hexonic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

(1R)-2,3;5,6-Di-O-isopropyliden-1-methylphosphono-1-O-tosyl-D-mannit-δ-phoston → 2-Desoxy-D-arabino-hexonsaeuremethylester (27963-68-4)

Guidance literature:

With sodium methylate; In methanol; for 0.25h;

Reference yield:

3,4,5,6-tetra-O-acetyl-1-deoxy-1-diazo-keto-D-fructose (14214-09-6) → 2-Desoxy-D-arabino-hexonsaeuremethylester (27963-68-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Ag₂O

2: NaOMe

With sodium methylate; silver(l) oxide;

Reference yield:

methanol (67-56-1) + Tetra-O-acetyl-2-deoxy-D-arabino-hexonsaeure-aethylester (27963-67-3) → 2-Desoxy-D-arabino-hexonsaeuremethylester (27963-68-4)

Guidance literature:

With sodium methylate;

upstream raw materials:

methanol

Tetra-O-acetyl-2-deoxy-D-arabino-hexonsaeure-aethylester

3,4,5,6-tetra-O-acetyl-1-deoxy-1-diazo-keto-D-fructose

Downstream raw materials:

3,4,5,6-Tetra-O-acetyl-2-desoxy-D-arabino-hexonsaeuremethylester

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