2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE

Base Information

Chemical Name:2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE
CAS No.:330435-58-0
Molecular Formula:C7H9F3O5S
Molecular Weight:262.2
Hs Code.:2932999099
Mol file:330435-58-0.mol

Synonyms:2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE

Suppliers and Price of 2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE 95.00%
5MG
$ 495.84

Total 1 raw suppliers

Chemical Property of 2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE

Chemical Property:

Boiling Point:263.2±40.0 °C(Predicted)
PSA：70.21000
Density:1.50±0.1 g/cm3(Predicted)
LogP:2.55770

Purity/Quality:: 2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE

There total 1 articles about 2,2-DIMETHYL-4H-1,3-DIOXIN-5-YL TRIFLUOROMETHANESULFONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 74181-34-3
2,2,-dimethyl-1,3-dioxan-5-one

: 330435-58-0
2,2-dimethyl-4H-1,3-dioxin-5-yl trifluoromethanesulfonate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -23 ℃; for 24h;
DOI:10.1016/S0040-4020(00)00872-3

Reference yield: 88.0%

: 40138-16-7
2-formylbenzene boronic acid

: 330435-58-0
2,2-dimethyl-4H-1,3-dioxin-5-yl trifluoromethanesulfonate

: 330435-61-5
2,2-dimethyl-5-(2-formylphenyl)-4H-1,3-dioxin

Guidance literature:: With bis(benzonitrile)palladium(II) dichloride; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 20 ℃; for 14h;
DOI:10.1016/S0040-4020(00)00872-3

Reference yield: 75.0%

: 960-16-7
tributylphenylstannane

: 330435-58-0
2,2-dimethyl-4H-1,3-dioxin-5-yl trifluoromethanesulfonate

: 330435-60-4
2,2-dimethyl-5-phenyl-4H-1,3-dioxin

Guidance literature:: 2,2-dimethyl-4H-1,3-dioxin-5-yl trifluoromethanesulfonate; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 0.166667h;

tributylphenylstannane; With Pd₂(dibenzylideneacetone)2*CHCl₃; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 50h;
DOI:10.1016/S0040-4020(00)00872-3