TriMethyl 2-broMobenzene-1,3,5-tricarboxylate

Base Information

• Chemical Name: TriMethyl 2-broMobenzene-1,3,5-tricarboxylate
• CAS No.: 43141-00-0
• Molecular Formula: C12H11BrO6
• Molecular Weight: 331.11614
• Mol file: 43141-00-0.mol

Synonyms:TriMethyl 2-broMobenzene-1,3,5-tricarboxylate

Chemical Property of TriMethyl 2-broMobenzene-1,3,5-tricarboxylate

Chemical Property:

• PSA: 78.90000
• LogP: 1.80890

Purity/Quality:

99% ^*data from raw suppliers

Trimethyl2-bromobenzene-1,3,5-tricarboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TriMethyl 2-broMobenzene-1,3,5-tricarboxylate

There total 2 articles about TriMethyl 2-broMobenzene-1,3,5-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.6%

methanol (67-56-1) + 2-Bromobenzene-1,3,5-tricarboxylic acid (13520-03-1) → Trimethyl 2-bromobenzene-1,3,5-tricarboxylate (43141-00-0)

Guidance literature:

With sulfuric acid; for 20h; Heating;

DOI:10.1135/cccc20010820

Reference yield:

2,4,6-trimethylphenyl bromide (576-83-0) → Trimethyl 2-bromobenzene-1,3,5-tricarboxylate (43141-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / aq. NaOH; KMnO₄ / 8 h / Heating

2: 84.6 percent / H₂SO₄ / 20 h / Heating

With sodium hydroxide; potassium permanganate; sulfuric acid;

DOI:10.1135/cccc20010820

Reference yield: 80.0%

aniline (62-53-3) + Trimethyl 2-bromobenzene-1,3,5-tricarboxylate (43141-00-0) → anilino-benzene-1,3,5-tricarboxylic acid trimethyl ester (132347-45-6)

Guidance literature:

In methanol; for 20h; Heating;

upstream raw materials:

methanol

2-Bromobenzene-1,3,5-tricarboxylic acid

2,4,6-trimethylphenyl bromide

Downstream raw materials:

anilino-benzene-1,3,5-tricarboxylic acid trimethyl ester

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