DDE-L-LYS(BOC)-OH

Base Information

Chemical Name:DDE-L-LYS(BOC)-OH
CAS No.:1189586-14-8
Molecular Formula:C21H34N2O6
Molecular Weight:410.5
Hs Code.:
Mol file:1189586-14-8.mol

Synonyms:DDE-L-LYS(BOC)-OH;DDE-LYS(BOC)-OH;N-ALPHA-1-(4,4-DIMETHYL-2,6-DIOXOCYCLOHEX-1-YLIDENE)ETHYL-N-EPSILON-BOC-L-LYSINE;N-ALPHA-(4,4-DIMETHYL-2,6-DIOXOCYCLOHEX-1-YLIDENE)ETHYL-N-EPSILON-T-BUTYLOXYCARBONYL-L-LYSINE;N-ALPHA-(4-4-DIMETHYL-2,6-DIOXOCYCLOHEX-1-YLIDENE)ETHYL-N-EPSILON-TERT-BUTYLOXYCARBONYL-L-LYSINE

Suppliers and Price of DDE-L-LYS(BOC)-OH

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Iris Biotech GmbH
Dde-L-Lys(Boc)-OH
25 g
$ 810.00

Iris Biotech GmbH
Dde-L-Lys(Boc)-OH
5 g
$ 202.50

Crysdot
(S)-6-((tert-Butoxycarbonyl)amino)-2-((1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl)amino)hexanoicacid 97%
1g
$ 89.00

Crysdot
(S)-6-((tert-Butoxycarbonyl)amino)-2-((1-(4,4-dimethyl-2,6-dioxocyclohexylidene)ethyl)amino)hexanoicacid 97%
5g
$ 238.00

Chem-Impex
Nα-1-(4,4-Dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl-Nε-Boc-L-lysine,98%(HPLC) 98%(HPLC)
1G
$ 56.00

Chem-Impex
Nα-1-(4,4-Dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl-Nε-Boc-L-lysine,≥98%(HPLC) ≥98%(HPLC)
5G
$ 221.31

Biosynth Carbosynth
N-alpha-1-(4,4-Dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl-Nepsilon-Boc-L-lysine
1 g
$ 83.60

Biosynth Carbosynth
N-alpha-1-(4,4-Dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl-Nepsilon-Boc-L-lysine
2 g
$ 133.70

Biosynth Carbosynth
N-alpha-1-(4,4-Dimethyl-2,6-dioxocyclohex-1-ylidene)ethyl-Nepsilon-Boc-L-lysine
5 g
$ 213.90

American Custom Chemicals Corporation
DDE-L-LYS(BOC)-OH 95.00%
1G
$ 760.00

Total 4 raw suppliers

Chemical Property of DDE-L-LYS(BOC)-OH

Chemical Property:

Boiling Point:591.8±50.0 °C(Predicted)
PKA:12.92±0.46(Predicted)
PSA：121.80000
Density:1.137±0.06 g/cm3(Predicted)
LogP:3.73820

Purity/Quality:

97% ^*data from raw suppliers

Dde-L-Lys(Boc)-OH ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of DDE-L-LYS(BOC)-OH

There total 4 articles about DDE-L-LYS(BOC)-OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1755-15-3
2-acetyldimedone

: 2418-95-3
(S)-2-amino-6-(tert-butoxycarbonylamino)hexanoic acid

: 1189586-14-8,1272754-98-9
Dde-Lys-OH

Guidance literature:: With triethylamine; In ethanol; for 18h; Reflux;
DOI:10.1021/acs.jmedchem.7b01280

Reference yield:

: 2418-95-3
(S)-2-amino-6-(tert-butoxycarbonylamino)hexanoic acid

: 94142-97-9
2-(1-hydroxyethylidene)-5,5-dimethylcyclohexane-1,3-dione

: 1189586-14-8,1272754-98-9
Dde-Lys-OH

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; at 35 ℃; Inert atmosphere;
DOI:10.1021/jm801481y

Reference yield:

: 126-81-8
dimedone

: 1189586-14-8,1272754-98-9
Dde-Lys-OH

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 8 h / 20 °C / Cooling with ice

2: triethylamine / ethanol / 18 h / Reflux

With dmap; triethylamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1021/acs.jmedchem.7b01280