N,N-dimethyl-4-(tributylstannyl)aniline

Base Information

Chemical Name:N,N-dimethyl-4-(tributylstannyl)aniline
CAS No.:84600-70-4
Molecular Formula:C20H37NSn
Molecular Weight:410.23
Hs Code.:2931200000
DSSTox Substance ID:DTXSID20448622
Mol file:84600-70-4.mol

Synonyms:84600-70-4;N,N-dimethyl-4-(tributylstannyl)aniline;N,N-dimethyl-4-tributylstannylaniline;[4-(Dimethylamino)phenyl]tributylstannane;Benzenamine, N,N-dimethyl-4-(tributylstannyl)-;SCHEMBL1451865;DTXSID20448622

Suppliers and Price of N,N-dimethyl-4-(tributylstannyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
N,N-Dimethyl-4-(tributylstannyl)aniline
1 g
$ 352.00

SynQuest Laboratories
N,N-Dimethyl-4-(tributylstannyl)aniline
250 mg
$ 120.00

Total 3 raw suppliers

Chemical Property of N,N-dimethyl-4-(tributylstannyl)aniline

Chemical Property:

Boiling Point:420.6±47.0 °C(Predicted)
PKA:5.15±0.24(Predicted)
PSA：3.24000
LogP:5.30670
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:11
Exact Mass:411.194803
Heavy Atom Count:22
Complexity:247

Purity/Quality:: N,N-Dimethyl-4-(tributylstannyl)aniline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C1=CC=C(C=C1)N(C)C

Technology Process of N,N-dimethyl-4-(tributylstannyl)aniline

There total 4 articles about N,N-dimethyl-4-(tributylstannyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 586-77-6
4-bromo-N,N-dimethylaniline

: 1067-52-3
tributyltin methoxide

: 84600-70-4
4-(N,N-dimethyl)-1-tributylstannylbenzene

Guidance literature:: With manganese; chloro-trimethyl-silane; (2,2'-bipyridine)nickel(II) dibromide; tetraethylammonium iodide; triphenylphosphine; In N,N-dimethyl-formamide; at 50 - 400 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c5ob01096a

Reference yield: 61.0%

: 586-77-6
4-bromo-N,N-dimethylaniline

: 1461-22-9
tributyltin chloride

: 84600-70-4
4-(N,N-dimethyl)-1-tributylstannylbenzene

Guidance literature:: With trifluoroacetic acid; cobalt(II) bromide; zinc; In acetonitrile; CoBr2 and Zn dust activated with CF3CO2H reacted for 5 min with allyl chloride in MeCN, aryl halide and tributylstannyl chloride added simultaneously in MeCN at room temp., stirred for 4 h at 50°C;
DOI:10.1039/b417326k

Reference yield:

: 698-70-4
4-Iodo-N,N-dimethylaniline

: 1461-22-9
tributyltin chloride

: 84600-70-4
4-(N,N-dimethyl)-1-tributylstannylbenzene

Guidance literature:: tributyltin chloride; With naphthalene; lithium; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

4-Iodo-N,N-dimethylaniline; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jacs.5b06587