1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Base Information

Chemical Name:1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester
CAS No.:33329-69-0
Molecular Formula:C13H21NO3
Molecular Weight:239.31
Hs Code.:
Mol file:33329-69-0.mol

Synonyms:1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester;2(1)-4,4,6-trimethyl-5,6-dihydro-1,3-oxazine

Suppliers and Price of 1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 3 raw suppliers

Chemical Property of 1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Chemical Property:

PSA：47.89000
LogP:1.75120

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

There total 3 articles about 1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.2%

: 107-41-5
2-methyl-2,4-pentanediol

: 1558-81-2
1-carbethoxy-1-cyanocyclopropane

: 33329-69-0
1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: With sulfuric acid; at 0 ℃; for 1h;

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 33329-69-0
1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Guidance literature:

Reference yield:

: 105-56-6
ethyl 2-cyanoacetate

: 33329-69-0
1-(4,4,6-trimethyl-5,6-dihydro-4H-[1,3]oxazin-2-yl)-cyclopropanecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammomium bromide; potassium carbonate / N,N-dimethyl-formamide / 80 °C

2: sulfuric acid / 1 h / 0 °C

With sulfuric acid; tetrabutylammomium bromide; potassium carbonate; In N,N-dimethyl-formamide;