p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside

Base Information

• Chemical Name: p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside
• CAS No.: 210418-04-5
• Molecular Formula: C₁₂H₁₄N₄O₇
• Molecular Weight: 326.266
• Mol file: 210418-04-5.mol

Synonyms:p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside;4-Nitrophenyl 2-azido-2-deoxy-α-D-galactopyranoside;4-Nitrophenyl 2-azido-2-deoxy-alpha-D-galactopyranoside

Chemical Property of p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside

Chemical Property:

• Melting Point: 170-172°C
• PSA: 174.72000
• LogP: 0.06746
• Storage Temp.: Refrigerator, Under Inert Atmosphere
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

p-Nitrophenyl2-Azido-2-deoxy-α-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: p-Nitrophenyl 2-Azido-2-deoxy-α-D-galactopyranoside (cas# 210418-04-5) is a compound useful in organic synthesis.

Technology Process of p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside

There total 3 articles about p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside (1147438-51-4) → C12H14N4O7 (210418-04-5)

Guidance literature:

p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside; With sodium methylate; In methanol; at 20 ℃; for 0.5h; pH=10;

In methanol;

DOI:10.1016/j.carres.2011.03.036

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → C12H14N4O7 (210418-04-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C

2.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

2.2: Dowex H+

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; In methanol; dichloromethane;

DOI:10.1016/j.carres.2011.03.036

Reference yield:

3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyltrichloroacetimidate (83025-20-1) → C12H14N4O7 (210418-04-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C

2.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

2.2: Dowex H+

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; In methanol; dichloromethane;

DOI:10.1016/j.carres.2011.03.036

upstream raw materials:

p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

4-nitro-phenol

3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyltrichloroacetimidate

Downstream raw materials:

p-nitrophenyl 2-azido-3-O-benzoyl-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

p-nitrophenyl 2-azido-3-O-benzoyl-2-deoxy-α-D-galactopyranoside

p-nitrophenyl 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1->3)-2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

p-nitrophenyl 2-acetamido-4,6-di-O-benzoyl-2,3-N,O-carbonyl-2-deoxy-β-D-glucopyranosyl-(1->3)-2-azido-2-deoxy-4,6-O-p-methoxybenzylidene-α-D-galactopyranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 210418-04-5 p-Nitrophenyl 2-Azido-2-deoxy-a-D-galactopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send