2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole

Base Information

• Chemical Name: 2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole
• CAS No.: 1312765-17-5
• Molecular Formula: C₁₀H₁₆BNO₃S
• Molecular Weight: 241.119
• Hs Code.: 2934999090
• Mol file: 1312765-17-5.mol

Synonyms:2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole;2-Methoxy-1,3-thiazole-5-boronic acid, pinacol ester;2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole, 2-(2-Methoxy-1,3-thiazol-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Chemical Property of 2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole

Chemical Property:

• PSA: 68.82000
• LogP: 1.45090

Purity/Quality:

97% ^*data from raw suppliers

2-Methoxy-1,3-thiazole-5-boronic acid, pinacol ester ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole

There total 1 articles about 2-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,3-thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-methoxythiazole (446287-05-4) + bis(pinacol)diborane (73183-34-3) → 2-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiazole (1312765-17-5)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 100 ℃; for 0.5h; Inert atmosphere;

Reference yield: 90.0%

2-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiazole (1312765-17-5) + N-(6-bromoisoquinolin-1-yl)-N-((4’-methoxy-3’-methyl-[1,1‘-biphenyl]-4-yl)methyl)-3,3-dimethylbutanamide → N-((4'-methoxy-3'-methyl-[1,1'-biphenyl]-4-yl)methyl)-N-(6-(2-methoxythiazol-5-yl)isoquinolin-1-yl)-3,3-dimethylbutanamide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 1h; Inert atmosphere;

Reference yield:

2-methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiazole (1312765-17-5) + C21H14F2IN7O → C25H18F2N8O2S

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; N,N-dimethyl-formamide; at 100 ℃; for 2.5h; Inert atmosphere;

upstream raw materials:

5-bromo-2-methoxythiazole

bis(pinacol)diborane

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