1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE

Base Information

Chemical Name:1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE
CAS No.:954123-46-7
Molecular Formula:C8H5Br2F3
Molecular Weight:317.931
Hs Code.:2903999090
Mol file:954123-46-7.mol

Synonyms:1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE;3-Bromo-5-(trifluoromethyl)benzyl bromide

Suppliers and Price of 1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1-Bromo-3-(bromomethyl)-5-(trifluoromethyl)benzene
500mg
$ 65.00

SynQuest Laboratories
3-Bromo-5-(trifluoromethyl)benzyl bromide
5 g
$ 288.00

American Custom Chemicals Corporation
3-BROMO-5-(TRIFLUOROMETHYL)BENZYL BROMIDE 95.00%
5MG
$ 505.25

Ambeed
1-Bromo-3-(bromomethyl)-5-(trifluoromethyl)benzene 95%
5g
$ 105.00

Ambeed
1-Bromo-3-(bromomethyl)-5-(trifluoromethyl)benzene 95%
1g
$ 36.00

Ambeed
1-Bromo-3-(bromomethyl)-5-(trifluoromethyl)benzene 95%
250mg
$ 15.00

Alichem
3-Bromo-5-(trifluoromethyl)benzylbromide
1g
$ 1490.00

Total 15 raw suppliers

Chemical Property of 1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE

Chemical Property:

Boiling Point:241℃
Flash Point:100℃
PSA：0.00000
Density:1.885
LogP:4.36280
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-Bromo-3-(bromomethyl)-5-(trifluoromethyl)benzene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE

There total 5 articles about 1-BROMO-3-(BROMOMETHYL)-5-(TRIFLUOROMETHYL)BENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 172023-97-1
(3‐bromo‐5‐(trifluoromethyl)phenyl)methanol

: 954123-46-7
1‐bromo‐3‐(bromomethyl)‐5‐(trifluoromethyl)benzene

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201903707

Reference yield:

: 328-80-3
3-nitro-5-trifluoromethyl-benzoic acid

: 954123-46-7
1‐bromo‐3‐(bromomethyl)‐5‐(trifluoromethyl)benzene

Guidance literature:: Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran

2: tert.-butylnitrite; copper(ll) bromide / acetonitrile

3: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran

With N-Bromosuccinimide; tert.-butylnitrite; borane-THF; triphenylphosphine; copper(ll) bromide; In tetrahydrofuran; acetonitrile; 2: |Sandmeyer Reaction;
DOI:10.1016/j.bmcl.2015.04.098

Reference yield:

: 537039-44-4
[3-amino-5-(trifluoromethyl)phenyl]methanol

: 954123-46-7
1‐bromo‐3‐(bromomethyl)‐5‐(trifluoromethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tert.-butylnitrite; copper(ll) bromide / acetonitrile

2: N-Bromosuccinimide; triphenylphosphine / tetrahydrofuran

With N-Bromosuccinimide; tert.-butylnitrite; triphenylphosphine; copper(ll) bromide; In tetrahydrofuran; acetonitrile; 1: |Sandmeyer Reaction;
DOI:10.1016/j.bmcl.2015.04.098