Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate

Base Information

• Chemical Name: Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate
• CAS No.: 353292-81-6
• Molecular Formula: C9H11NO4
• Molecular Weight: 197.191
• European Community (EC) Number: 834-808-7
• Mol file: 353292-81-6.mol

Synonyms:353292-81-6;Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate;ethyl 2-(3-hydroxypyridin-2-yloxy)acetate;ethyl 2-(3-hydroxypyridin-2-yl)oxyacetate;ethyl 2-[(3-hydroxypyridin-2-yl)oxy]acetate;Ethyl [(3-hydroxy-2-pyridinyl)oxy]acetate;3-hydroxy-2-(ethoxycarbonyl)methoxypyridine;ethyl ((3-hydroxy-2-pyridinyl)oxy)acetate;SCHEMBL5593086;ABMQGSICTIPMKL-UHFFFAOYSA-N;Acetic acid, [(3-hydroxy-2-pyridinyl)oxy]-, ethyl ester (9CI);SB54488;Ethyl2-((3-hydroxypyridin-2-yl)oxy)acetate;G47087;EN300-4521987;Z1862010166

Chemical Property of Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate

Chemical Property:

• Boiling Point: 169 °C (3.0003 mmHg)
• PSA: 68.65000
• LogP: 0.72910
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 197.06880783
• Heavy Atom Count: 14
• Complexity: 186

Purity/Quality:

98%+ ^*data from raw suppliers

Ethyl2-((3-hydroxypyridin-2-yl)oxy)acetate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)COC1=C(C=CC=N1)O

Technology Process of Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate

There total 2 articles about Ethyl 2-((3-hydroxypyridin-2-yl)oxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dihydroxypyridine (16867-04-2) + ethyl diazoacetate → ethyl 2-((3- hydroxypyridin-2-yl)oxy)acetate (353292-81-6)

Guidance literature:

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 85 ℃;

Reference yield:

3-acetoxy-2-(ethoxycarbonyl)methoxypyridine (353293-55-7) → ethyl 2-((3- hydroxypyridin-2-yl)oxy)acetate (353292-81-6)

Guidance literature:

With hydrogenchloride; sodium chloride; potassium carbonate; In ethanol; water;

Reference yield: 57.0%

ethyl 2-((3- hydroxypyridin-2-yl)oxy)acetate (353292-81-6) + 4-(difluoromethyl)-2-(2,5-difluoro-4-nitro-phenyl)-5-methyl-1,2,4-triazol-3-one → ethyl 2-[[3-[5-[4-(difluoromethyl)-3-methyl-5-oxo-1,2,4-triazol-1-yl]-4-fluoro-2-nitro-phenoxy]-2-pyridyl]oxy]acetate

Guidance literature:

With caesium carbonate; In tetrahydrofuran; for 4h; Reflux;

upstream raw materials:

3-acetoxy-2-(ethoxycarbonyl)methoxypyridine

dihydroxypyridine

Downstream raw materials:

3-{4-fluoro-5-[3-methyl-2,6-dioxo-4-(trifluoromethyl)-1,2,3,6-tetrahydropyrimidin-1-yl]-2-nitrophenoxy}-2-(ethoxycarbonyl)methoxypyridine

[3-(2-chloro-4-nitro-phenoxy)-pyridin-2-yloxy]-acetic acid ethyl ester

[3-(4-fluoro-2-nitro-phenoxy)-pyridin-2-yloxy]-acetic acid ethyl ester

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