2-(4-benzylMorpholin-2-yl)ethan-1-aMine

Base Information

• Chemical Name: 2-(4-benzylMorpholin-2-yl)ethan-1-aMine
• CAS No.: 112914-08-6
• Molecular Formula: C13H20N2O
• Molecular Weight: 220.315
• Hs Code.: 2934999090
• Mol file: 112914-08-6.mol

Synonyms:2-(4-benzylMorpholin-2-yl)ethan-1-aMine;2-(4-Benzylmorpholin-2-yl)ethanamine;4-Benzyl-2-morpholineethanamine

Chemical Property of 2-(4-benzylMorpholin-2-yl)ethan-1-aMine

Chemical Property:

• Boiling Point: 327.9±22.0 °C(Predicted)
• PKA: 9.90±0.10(Predicted)
• PSA: 38.49000
• Density: 1.058±0.06 g/cm3(Predicted)
• LogP: 1.87440
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Benzyl-2-morpholineethanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(4-benzylMorpholin-2-yl)ethan-1-aMine

There total 8 articles about 2-(4-benzylMorpholin-2-yl)ethan-1-aMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(4-benzylmorpholin-2-yl)acetonitrile (57962-45-5) → 2-(2-aminoethyl)-4-benzylmorpholine (112914-08-6)

Guidance literature:

With ammonium hydroxide; hydrogen; nickel; In ethanol; Ambient temperature;

DOI:10.1021/jm00167a020

Reference yield:

ammonium hydroxide + (4-benzylmorpholin-2-yl)acetonitrile (57962-45-5) + maleic acid (110-16-7,26099-09-2) → sesquimaleate + 2-(2-aminoethyl)-4-benzylmorpholine (112914-08-6)

Guidance literature:

aluminum nickel; In ethanol;

Reference yield:

N-benzyl-2-chloromethylmorpholine (40987-25-5,186293-54-9) → 2-(2-aminoethyl)-4-benzylmorpholine (112914-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 93 percent / potassium iodide / dimethylsulfoxide / 5 h / 120 °C

2: 81 percent / 28percent ammonia water, H₂ / Raney nickel / ethanol / Ambient temperature

With ammonium hydroxide; hydrogen; potassium iodide; nickel; In ethanol; dimethyl sulfoxide;

DOI:10.1021/jm00167a020

upstream raw materials:

N-<2-(4-benzyl-2-morpholinyl)ethyl>phthalimide

(4-benzylmorpholin-2-yl)acetonitrile

2-(2-hydroxyethyl)-4-benzylmorpholine

2-(2-chloroethyl)-4-(phenylmethyl)morpholine

Downstream raw materials:

4-amino-N-[2-(4-benzyl-2-morpholinyl)ethyl]-5-chloro-2-methoxybenzamide

4-amino-N-[2-(4-benzyl-2-morpholinyl)ethyl]-5-chloro-2-ethoxybenzamide

C₁₅H₁₉F₃N₂O₂

N-[2-(4-Benzyl-2-morpholinyl)ethyl]-5-(1,2-dithiolan-3-yl)pentane Thioamide

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