Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)-

Base Information

• Chemical Name: Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)-
• CAS No.: 4549-20-6
• Molecular Formula: C8H15N3O
• Molecular Weight: 169.227
• Hs Code.: 2928000090
• NSC Number: 6856
• DSSTox Substance ID: DTXSID10418733
• Nikkaji Number: J119.641C
• Mol file: 4549-20-6.mol

Synonyms:NSC6856;4549-20-6;Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)-;Cyclohexanone, 2-methyl-, semicarbazone;DTXSID10418733;2-Methylcyclohexanone semicarbazone;NSC-6856

Chemical Property of Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)-

Chemical Property:

• Melting Point: 188-189.5 °C
• Boiling Point: °Cat760mmHg
• PKA: 12.32±0.40(Predicted)
• Flash Point: °C
• PSA: 67.48000
• Density: 1.24g/cm³
• LogP: 2.31200
• XLogP3: 0.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 169.121512110
• Heavy Atom Count: 12
• Complexity: 201

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CCCCC1=NNC(=O)N
• Isomeric SMILES: CC\1CCCC/C1=N/NC(=O)N

Technology Process of Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)-

There total 10 articles about Hydrazinecarboxamide, 2-(2-methylcyclohexylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methylcyclohexanol (583-59-5) → 2-methyl cyclohexanone semicarbazone (4549-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: CrO₃; aqueous acetic acid

With chromium(VI) oxide; acetic acid;

DOI:10.1039/jr9420000121

Reference yield:

2-Chlorocyclohexanone (822-87-7) → 2-methyl cyclohexanone semicarbazone (4549-20-6)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether / anschliessende Behandlung mit wss. H₂SO₄

2: water / 200 °C

With diethyl ether; water;

DOI:10.1021/ja01324a046

Reference yield:

2-chloro-1-methylcyclohexanol (19324-75-5,60537-96-4,75908-24-6,142282-82-4) → 2-methyl cyclohexanone semicarbazone (4549-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: water / 200 °C

With water;

DOI:10.1021/ja01324a046

upstream raw materials:

ethanol

2-Methylcyclohexanone

1-vinyl-1-cyclopentanol

hydrazine carboxamide

Downstream raw materials:

hydrazodicarboxamide

2-methylcyclohexanone phenylhydrazone

2-Methylcyclohexanone

Cr(OC(NH₂)NHN(C₆H₉(CH₃)))2Cl₂⁽¹⁺⁾*Cl^(1-)=Cr(OC(NH₂)NHN(C₆H₉(CH₃)))2Cl₃