Cyclohexanone, 2-methyl-, phenylhydrazone

Base Information

• Chemical Name: Cyclohexanone, 2-methyl-, phenylhydrazone
• CAS No.: 1208-57-7
• Molecular Formula: C13H18N2
• Molecular Weight: 202.299
• Mol file: 1208-57-7.mol

Synonyms:

Chemical Property of Cyclohexanone, 2-methyl-, phenylhydrazone

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexanone, 2-methyl-, phenylhydrazone

There total 3 articles about Cyclohexanone, 2-methyl-, phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl cyclohexanone semicarbazone (4549-20-6) + phenylhydrazine (100-63-0) + toluene (108-88-3,15644-74-3,16713-13-6) → hydrazodicarboxamide (110-21-4) + 1-(2-methyl-cyclohexylidene)-5-phenyl carbonohydrazide + 2-methylcyclohexanone phenylhydrazone (1208-57-7)

Guidance literature:

at 130 - 135 ℃;

Reference yield:

2-Methylcyclohexanone (583-60-8) + phenylhydrazine (100-63-0) → 2-methylcyclohexanone phenylhydrazone (1208-57-7)

Guidance literature:

In methanol; for 0.25h; Ambient temperature;

DOI:10.1055/s-1990-27022

Reference yield:

→ 2-methylcyclohexanone phenylhydrazone (1208-57-7)

Guidance literature:

2-Methylcyclohexanon, Phenylhydrazin;

DOI:10.1002/jps.2600651119

upstream raw materials:

2-methyl cyclohexanone semicarbazone

phenylhydrazine

toluene

2-Methylcyclohexanone

Downstream raw materials:

4a-methyl-2,3,4,4a-tetrahydro-1H-carbazole

4a,8-dimethyl-2,3,4,4a-tetrahydro-1H-carbazole

9H-carbazole

1-methyl-9H-carbazole

Refernces

• 1、 Okimoto, Mitsuhiro,Takahashi, Yukio,Kakuchi, Toyoji. "Electrochemical formation of methoxy- and cyano(phenylazo)alkanes from aldehyde and ketone phenylhydrazones". . p. 2057 - 2063. Retrieved 2007/10/03.
• 2、 Gstach, Hubert,Seil, Patrick. "Rearrangement of 3,3-Disubstituted 1-Aryl-4,5-dihydro-5-oxo-3H-1,2,4-triazolium Tetrafluoroborates; Part 2. A Convenient Synthesis of 1,5-Annulated 1,2-Dihydro-2-phenyl-3H-1,2,4-triazol-3-ones". . p. 808 - 815. Retrieved 2007/10/02.