3-Bomo-4-pridinepropanoic acidethylester

Base Information

Chemical Name:3-Bomo-4-pridinepropanoic acidethylester
CAS No.:463303-98-2
Molecular Formula:C10H12BrNO2
Molecular Weight:258.11178
Hs Code.:2933399090
Mol file:463303-98-2.mol

Synonyms:3-Bomo-4-pridinepropanoic acidethylester;4-Pyridinepropanoic acid, 3-broMo-, ethyl ester

Suppliers and Price of 3-Bomo-4-pridinepropanoic acidethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Ethyl3-(3-bromopyridin-4-yl)propanoate 95+%
1g
$ 1305.00

Chemenu
ethyl3-(3-bromopyridin-4-yl)propanoate 95%
1g
$ 1230.00

American Custom Chemicals Corporation
ETHYL-3-(3-BROMOPYRIDIN-4-YL)PROPANOATE 95.00%
5MG
$ 501.90

Alichem
Ethyl3-(3-bromopyridin-4-yl)propanoate
1g
$ 1077.12

Total 11 raw suppliers

Chemical Property of 3-Bomo-4-pridinepropanoic acidethylester

Chemical Property:

PSA：39.19000
LogP:2.33980
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl3-(3-bromopyridin-4-yl)propanoate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Bomo-4-pridinepropanoic acidethylester

There total 3 articles about 3-Bomo-4-pridinepropanoic acidethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-36-2
ethyl bromoacetate

: 3430-22-6
3-Bromo-4-methylpyridin

: 463303-98-2
3-(3-bromo-4-pyridyl)propionic acid ethyl ester

Guidance literature:: 3-Bromo-4-methylpyridin; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

ethyl bromoacetate; In tetrahydrofuran; for 2h;

Reference yield:

: 6414-69-3
ethyl 3-iodopropanoate

: 92915-13-4
3-bromopyridinium ethylformate chloride

: 463303-98-2
3-(3-bromo-4-pyridyl)propionic acid ethyl ester

Guidance literature:: ethyl 3-iodopropanoate; With lithium chloride; zinc; In tetrahydrofuran; at -50 ℃;

3-bromopyridinium ethylformate chloride; In tetrahydrofuran; at -40 - 0 ℃;

With sulfur; In xylene; for 72h; Further stages.; Heating;
DOI:10.1021/jm020916b

Reference yield:

: 626-55-1,163928-56-1
3-Bromopyridine

: 463303-98-2
3-(3-bromo-4-pyridyl)propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 1 h / 0 °C

2.1: Zn; LiCl; CuCN / tetrahydrofuran / -50 °C

2.2: tetrahydrofuran / -40 - 0 °C

2.3: sulfur / xylene / 72 h / Heating

With lithium chloride; zinc; In tetrahydrofuran; 2.2: Knochel reaction;
DOI:10.1021/jm020916b