2-[1-(4-Bromoanilino)ethylidene]malononitrile

Base Information

Chemical Name:2-[1-(4-Bromoanilino)ethylidene]malononitrile
CAS No.:360062-16-4
Molecular Formula:C11H8BrN3
Molecular Weight:262.11
Hs Code.:2926909090
DSSTox Substance ID:DTXSID80355141
Mol file:360062-16-4.mol

Synonyms:360062-16-4;2-[1-(4-bromoanilino)ethylidene]malononitrile;2-[1-(4-bromoanilino)ethylidene]propanedinitrile;2-(1-((4-Bromophenyl)amino)ethylidene)malononitrile;AH-262/36519027;DTXSID80355141;AKOS006223903;SR-01000201646;SR-01000201646-1

Suppliers and Price of 2-[1-(4-Bromoanilino)ethylidene]malononitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(1-[(4-BROMOPHENYL)AMINO]ETHYLIDENE)MALONONITRILE 95.00%
5MG
$ 495.14

Total 2 raw suppliers

Chemical Property of 2-[1-(4-Bromoanilino)ethylidene]malononitrile

Chemical Property:

Vapor Pressure:1.94E-05mmHg at 25°C
Boiling Point:362.4°C at 760 mmHg
Flash Point:173°C
PSA：59.61000
Density:1.532g/cm³
LogP:3.25516
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:260.99016
Heavy Atom Count:15
Complexity:329

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

(1-[(4-BROMOPHENYL)AMINO]ETHYLIDENE)MALONONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C(C#N)C#N)NC1=CC=C(C=C1)Br

Technology Process of 2-[1-(4-Bromoanilino)ethylidene]malononitrile

There total 3 articles about 2-[1-(4-Bromoanilino)ethylidene]malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 352554-18-8
(Z)-3-(4-Bromo-phenylamino)-2-cyano-but-2-enoic acid amide

: 360062-16-4
2-[1-(4-bromo-phenylamino)-ethylidene]-malononitrile

Guidance literature:: With trichlorophosphate; In acetonitrile; for 2h; Heating;
DOI:10.1023/A:1017566212124

Reference yield:

: 62321-92-0
α-cyano-β-dimethylaminocrotonamide

: 360062-16-4
2-[1-(4-bromo-phenylamino)-ethylidene]-malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / POCl₃ / acetonitrile / 2 h / Heating

With trichlorophosphate; In acetonitrile;
DOI:10.1023/A:1017566212124

Reference yield:

: 106-40-1
4-bromo-aniline

: 360062-16-4
2-[1-(4-bromo-phenylamino)-ethylidene]-malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / POCl₃ / acetonitrile / 2 h / Heating

With trichlorophosphate; In acetonitrile;
DOI:10.1023/A:1017566212124