14-Acetyldelcosine

Base Information

Chemical Name:14-Acetyldelcosine
CAS No.:50676-21-6
Molecular Formula:C26H41NO8
Molecular Weight:495.61
Hs Code.:
Mol file:50676-21-6.mol

Synonyms:14-Acetyldelcosine;20-Ethyl-6β,16β-dimethoxy-4-(methoxymethyl)aconitane-1α,7,8,14α-tetrol 14-acetate;Acetyldelcosine

Suppliers and Price of 14-Acetyldelcosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 14-Acetyldelcosine

Chemical Property:

PSA：117.92000
LogP:0.12560

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 14-Acetyldelcosine

There total 2 articles about 14-Acetyldelcosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: C₂₆H₃₉NO₈

: 50676-21-6
14-O-acetyldelcosine

: 14-acetyl-1-epi-delcosine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 1.83333h;
DOI:10.1248/cpb.48.660

Reference yield:

: 64-19-7,77671-22-8
acetic acid

: 545-56-2,6835-87-6,1356-55-4,22091-01-6,56596-01-1,7097-12-3
delcosine

: 50676-21-6
14-O-acetyldelcosine

Guidance literature:: With trifluoroacetic acid; at 80 - 90 ℃;
DOI:10.1139/v54-098

Reference yield:

: 50676-21-6
14-O-acetyldelcosine

: 545-56-2,6835-87-6,1356-55-4,22091-01-6,56596-01-1,7097-12-3
delcosine

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / pyridinium dichromate / CH₂Cl₂ / 5 h / 0 °C

2: 36 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

With lithium aluminium tetrahydride; dipyridinium dichromate; In tetrahydrofuran; dichloromethane; 1: Oxidation / 2: Reduction;
DOI:10.1248/cpb.48.660